SEM and TEM morphology imaging
Ni-HHTP comparative sample set · Unknown
Time-dependent SEM for electrosynthesis, SEM/TEM images of flower, disc and bulk morphologies.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| Bulk Ni-HHTP morphology | Rod-shaped bulk Ni-HHTP observed by SEM | — | — | Caption Qualitative | S13 · Structural Characterizations · Figure S11 |
| Disc dense stacked morphology | Circular plates in Ni-HHTP-Disc are dense and stacked, shielding portions from electrolyte | — | — | Text Qualitative | 52 · Results |
| Disc morphology stabilisation | Ni-HHTP-Disc shows small round crystallites after 30 min and no significant change after 1 h | — | — | Text Qualitative | 51 · Results · Figure 2c |
| Flower lamellar/free-space morphology | Free space between Ni-HHTP-Flower petals allows 2D Ni-HHTP to remain accessible | — | — | Text Qualitative | 52 · Results |
| Flower morphology fully grown | Ni-HHTP-Flower nanoparticles fully grown after 2 h | — | — | Text Exact Reported | 51 · Results · Figure 2b |
| Flower growth at 30 min | Small circular crystallites after 30 min | — | — | Text Qualitative | 51 · Results · Figure 2b |