Porosity — Electrosynthesis of a Nickel-Based Conductive Metal-Organic Framework with Controlled Morphology for Enhanced Capacitance

3 measurement groups · 9 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Solvothermal bulk Ni-HHTP powder/pellet · Pellet

BET surface area and pore size measured with Micromeritics ASAP 2020 PLUS; N2 sorption isotherm at 77 K.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Approximate N2 uptake at P/P0 near 1: bulk	approx. 190 cm3 g^-1 STP at P/P0 ~1	—	—	Figure Axis Approximate	S15 · Structural Characterizations · Figure S15a
Bulk absence of flower-like large mesopores	Mesopores >100 A not observed in rod-shaped bulk Ni-HHTP	—	—	Text Qualitative	53 · Results · Figures S15-S16
Approximate dominant pore width: bulk	dominant DFT pore-size peaks around 18-20 A	—	—	Figure Axis Approximate	S15 · Structural Characterizations · Figure S16a

Detached Ni-HHTP-Disc powder/pellet · Pellet

BET surface area and pore size measured with Micromeritics ASAP 2020 PLUS; N2 sorption isotherm at 77 K.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Approximate N2 uptake at P/P0 near 1: disc	approx. 135 cm3 g^-1 STP at P/P0 ~1	—	—	Figure Axis Approximate	S15 · Structural Characterizations · Figure S15c
Disc absence of flower-like large mesopores	Mesopores >100 A not observed in Ni-HHTP-Disc	—	—	Text Qualitative	53 · Results · Figures S15-S16
Approximate dominant pore width: disc	dominant DFT pore-size peak around 18-20 A	—	—	Figure Axis Approximate	S15 · Structural Characterizations · Figure S16c

Detached Ni-HHTP-Flower powder/pellet · Pellet

BET surface area and pore size measured with Micromeritics ASAP 2020 PLUS; N2 sorption isotherm at 77 K.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Approximate N2 uptake at P/P0 near 1: flower	approx. 300 cm3 g^-1 STP at P/P0 ~1	—	—	Figure Axis Approximate	S15 · Structural Characterizations · Figure S15b
Approximate flower broad mesopore widths	flower pore distribution includes broad features around 100-145 A	—	—	Figure Axis Approximate	S15 · Structural Characterizations · Figure S16b
Flower mesopore distributionMarked as a best value within this paper	Several mesopores greater than 100 A observed	—	—	Text Range	53 · Results · Figures S15-S16