Microscopy Morphology — Highly Conductive 2D Metal-Organic Framework Thin Film Fabricated by Liquid-Liquid Interfacial Reaction Using One-Pot-Synthesized Benzenehexathiol

Measurement evidence

Microscopy Morphology

Highly Conductive 2D Metal-Organic Framework Thin Film Fabricated by Liquid-Liquid Interfacial Reaction Using One-Pot-Synthesized Benzenehexathiol · Chen I.-F., Lu C.-F., Su W.-F. · Langmuir · 2018 · 15754-15762

2 measurement groups · 8 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

SEM surface imaging

Ag3BHT2 thin film · Thin Film

SEM surface images of thin and thick films; samples first covered with 5 nm platinum.

Geometry
SEM
Context
all pristine MOF samples
Measurement source
15760-15761 · Materials Characterization; Experimental Methods · Figure 7
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Ag3BHT2 thick film SEM morphologylarger roughness than thin film but large-scale continuous structureText
Qualitative
15760 · Materials Characterization · Figure 7b
Ag3BHT2 thin film SEM morphologyflat with cracks and small particles on the surfaceText
Qualitative
15760 · Materials Characterization · Figure 7a
Au3BHT2 thick film SEM morphologycracked and discontinuous, domains 10 to 100 umText
Qualitative
15760 · Materials Characterization · Figure 7d
Au3BHT2 thin film SEM morphologyextremely uniform without micrometer-scaled poresText
Qualitative
15760 · Materials Characterization · Figure 7c

SEM cross-sectional thickness measurement

Ag3BHT2 thin film · Thin Film

Film thickness determined from SEM cross-sectional images; thin films measured with NOVA NANO SEM 450 and thick films with JEOL JSM6510.

Geometry
cross-sectional SEM
Context
all pristine MOF samples
Measurement source
15761 · Materials Characterization · Table 2; Figures S5-S6
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Ag3BHT2 thick film thickness64.23 +/- 0.43 um+/- 0.43Table
Exact Reported
15759 · Materials Characterization · Table 2
Ag3BHT2 thin film thickness276.51 +/- 5.53 nm+/- 5.53Table
Exact Reported
15759 · Materials Characterization · Table 2
Au3BHT2 thick film thickness89.05 +/- 0.12 um+/- 0.12Table
Exact Reported
15759 · Materials Characterization · Table 2
Au3BHT2 thin film thickness324.72 +/- 11.23 nm+/- 11.23Table
Exact Reported
15759 · Materials Characterization · Table 2