Microscopy Morphology — Hybrid metal-organic chalcogenide nanowires with electrically conductive inorganic core through diamondoid-directed assembly

2 measurement groups · 4 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

As-synthesised 1ADCu needle-shaped crystals · Single Crystal

SEM on crystals lifted from interface and deposited on silicon; Au sputter coating for SEM; AFM after IPA dispersion and spin-casting.

Atmosphere: Air-dried before SEM/AFM.
Context: Pristine bulk crystals.
Measurement source: main p.2 and Methods · Fig. 1 caption; Characterizations · Fig. 1b

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
1ADCu crystal diameter upper bound	20 um	—	—	Text Rounded Reported	main p.1, article p.349 · Article text · Fig. 1b
1ADCu crystal diameter lower bound	10 nm	—	—	Text Rounded Reported	main p.1, article p.349 · Article text · Fig. 1b
1ADCu crystal length	>100 um	—	—	Text Approximate	main p.1, article p.349 · Article text · Fig. 1b

Ag-, Cd-, Zn- and Fe-based demonstration MOC crystals · Powder

SEM micrographs of non-copper MOC crystals and PXRD patterns of silver thiolate MOCs with different SDAs.

Temperature: room temperature for PXRD
Context: Pristine demonstration MOC crystals.
Measurement source: main p.6, article p.354 · Generality of synthesis · Fig. 6; Fig. S11-S12

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Ag [121]tetramantane-6-thiolate morphology tunable by solvent composition	Addition of ethanol to toluene generated thinner diameter 1D crystals	—	—	Text Qualitative	main p.6, article p.354 · Generality of synthesis · Fig. S12