Microscopy Morphology — In-Plane Oriented Two-Dimensional Conjugated Metal-Organic Framework Films for High-Performance Humidity Sensing

4 measurement groups · 12 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

free-standing in-plane oriented HIB-Cu film · Thin Film

FESEM, Carl Zeiss Gemini, 1-3 kV.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
EDX C atomic ratio in HIB-Cu film	C:N:Cu = 46:43:11	—	—	Text Rounded Reported	1148 · Results · Figure S2
EDX Cu atomic ratio in HIB-Cu film	C:N:Cu = 46:43:11	—	—	Text Rounded Reported	1148 · Results · Figure S2
EDX N atomic ratio in HIB-Cu film	C:N:Cu = 46:43:11	—	—	Text Rounded Reported	1148 · Results · Figure S2

free-standing in-plane oriented HIB-Cu film · Thin Film

FEI Titan 80-300 microscope, 300 kV.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
average HIB-Cu crystallite domain size with SDS	1691.3 +/- 802.3 nm2	—	+/- 802.3 nm2	Text Exact Reported	1149 · Results · Figure S6
maximum HIB-Cu crystal domain size with SDS	up to ~3000 nm2	—	—	Text Approximate	1151 · Summary · Figure S6
HIB-Cu pore size	~1 nm	—	—	Text Approximate	1149 · Results · Figure 3g

free-standing in-plane oriented HIB-Cu film · Thin Film

Thickness of HIB-Cu film varied with HAB concentration.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
HIB-Cu thickness at 1.25 mM HAB	54 +/- 14 nm	—	+/- 14 nm	Figure Axis Rounded Reported	1148 · Results · Figure 2c
HIB-Cu thickness at 2.5 mM HAB	119 +/- 8 nm	—	+/- 8 nm	Figure Axis Rounded Reported	1148 · Results · Figure 2c
HIB-Cu thickness at 3.75 mM HAB	343 +/- 16 nm	—	+/- 16 nm	Figure Axis Rounded Reported	1148 · Results · Figure 2c
tunable HIB-Cu film thickness range	50-340 nm	—	—	Text Range	1148 · Results · Figure 2c

HIB-Cu film made without SDS · Thin Film

Contrast experiment without SDS.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
amorphous areal fraction without SDS	35.83%	0.3583 fraction	—	Caption Exact Reported	12 · Supporting Figure S7 · Figure S7
average HIB-Cu crystallite size without SDS	204.3 +/- 96.8 nm2	—	+/- 96.8 nm2	Text Exact Reported	1149 · Results · Figure S6