Microscopy Morphology — Oxidative control over the morphology of Cu3(HHTP)2, a 2D conductive metal-organic framework

3 measurement groups · 9 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Cu3(HHTP)2 blocks, 0.3 equiv 2,5-dichloro pre-oxidant · Powder

SEM images and length/diameter distributions; over 250 particles analysed for rods in main text.

Atmosphere: air after synthesis
Context: pristine framework powder
Measurement source: p003-p005 / article pp.10474-10476 · Results and discussion · Figure 3

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
average particle length	0.55 +/- 0.33 um	—	+/- 0.33 um	Text Rounded Reported	p005 / article p.10476 · Results and discussion · Figure 3
average particle diameter	0.33 +/- 0.18 um	—	+/- 0.18 um	Text Rounded Reported	p005 / article p.10476 · Results and discussion · Figure 3
length:diameter aspect ratio	1.67	—	—	Text Rounded Reported	p005 / article p.10476 · Results and discussion · Figure 3

Cu3(HHTP)2 flakes, 0.5 equiv 2,5-dichloro pre-oxidant · Powder

SEM images and length/diameter distributions; over 250 particles analysed for rods in main text.

Atmosphere: air after synthesis
Context: pristine framework powder
Measurement source: p003-p005 / article pp.10474-10476 · Results and discussion · Figure 3

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
average particle length	0.06 +/- 0.02 um	—	+/- 0.02 um	Text Rounded Reported	p005 / article p.10476 · Results and discussion · Figure 3
average particle diameter	0.45 +/- 0.19 um	—	+/- 0.19 um	Text Rounded Reported	p005 / article p.10476 · Results and discussion · Figure 3
length:diameter aspect ratio	0.13	—	—	Text Rounded Reported	p005 / article p.10476 · Results and discussion · Figure 3

Cu3(HHTP)2 rods, 0 equiv pre-oxidant · Powder

SEM images and length/diameter distributions; over 250 particles analysed for rods in main text.

Atmosphere: air after synthesis
Context: pristine framework powder
Measurement source: p003-p005 / article pp.10474-10476 · Results and discussion · Figure 3

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
average particle length	1.15 +/- 0.8 um	—	+/- 0.8 um	Text Rounded Reported	p005 / article p.10476 · Results and discussion · Figure 3
average particle diameter	0.13 +/- 0.05 um	—	+/- 0.05 um	Text Rounded Reported	p005 / article p.10476 · Results and discussion · Figure 3
length:diameter aspect ratioMarked as a best value within this paper	8.85	—	—	Text Rounded Reported	p005 / article p.10476 · Results and discussion · Figure 3