Measurement evidence
Oxidative control over the morphology of Cu3(HHTP)2, a 2D conductive metal-organic framework · Snook K.M., Zasada L.B., Chehada D. et al. · Chemical Science · 2022 · 10472-10478
Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.
Cu3(HHTP)2 air-synthesis particles · Powder
Samples activated under dynamic vacuum at 80 deg C for 20 h; N2 adsorption at 77 K; BET range 0.02-0.09 P/P0.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| BET surface area | 563.9355 +/- 2.2252 m2/g | — | +/- 2.2252 m2/g | SI Table Exact Reported | S15 · Supplementary Tables · Table S8 |
| BET correlation coefficient R2 | 0.9999845 | — | — | SI Table Exact Reported | S15 · Supplementary Tables · Table S8 |
Cu3(HHTP)2 air-synthesis rods · Powder
Samples activated under dynamic vacuum at 80 deg C for 20 h; N2 adsorption at 77 K; BET range 0.02-0.09 P/P0.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| BET surface area | 517.3851 +/- 1.9405 m2/g | — | +/- 1.9405 m2/g | SI Table Exact Reported | S15 · Supplementary Tables · Table S8 |
| BET correlation coefficient R2 | 0.9999649 | — | — | SI Table Exact Reported | S15 · Supplementary Tables · Table S8 |
| BET surface area from Fig. S22 caption | 590 m2/g | — | — | Caption Rounded Reported | S32 · Supplementary Figures · Figure S22 |
Cu3(HHTP)2 blocks, 0.3 equiv 2,5-dichloro pre-oxidant · Powder
Samples activated under dynamic vacuum at 80 deg C for 20 h; N2 adsorption at 77 K; BET range 0.02-0.09 P/P0.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| BET surface area | 536.1005 +/- 2.3787 m2/g | — | +/- 2.3787 m2/g | SI Table Exact Reported | S15 · Supplementary Tables · Table S8 |
| BET correlation coefficient R2 | 0.9999705 | — | — | SI Table Exact Reported | S15 · Supplementary Tables · Table S8 |
| BET surface area from Fig. S22 caption | 680 m2/g | — | — | Caption Rounded Reported | S32 · Supplementary Figures · Figure S22 |
Cu3(HHTP)2 flakes, 0.5 equiv 2,5-dichloro pre-oxidant · Powder
Samples activated under dynamic vacuum at 80 deg C for 20 h; N2 adsorption at 77 K; BET range 0.02-0.09 P/P0.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| BET surface area | 385.0867 +/- 1.296 m2/g | — | +/- 1.296 m2/g | SI Table Exact Reported | S15 · Supplementary Tables · Table S8 |
| BET correlation coefficient R2 | 0.999983 | — | — | SI Table Exact Reported | S15 · Supplementary Tables · Table S8 |
Cu3(HHTP)2 rods, 0 equiv pre-oxidant · Powder
Samples activated under dynamic vacuum at 80 deg C for 20 h; N2 adsorption at 77 K; BET range 0.02-0.09 P/P0.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| BET surface areaMarked as a best value within this paper | 560.8445 +/- 2.6198 m2/g | — | +/- 2.6198 m2/g | SI Table Exact Reported | S15 · Supplementary Tables · Table S8 |
| BET correlation coefficient R2 | 0.9999673 | — | — | SI Table Exact Reported | S15 · Supplementary Tables · Table S8 |