Diffraction Structure — Large-Area Metal–Organic Framework Glasses for Efficient X-Ray Detection

3 measurement groups · 4 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Ag/ZnPIm/Ag planar MOF glass detector · Electrode

ZnPIm MOF glass measured before and after X-ray experiment.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
PXRD before/after X-ray exposure	No observable or detectable PXRD changes before and after X-ray exposure; glassy amorphous state retained.	—	—	Text Qualitative	correction p.1 · Correction · Figure S16

Dry ZnPIm powder · Powder

Freshly synthesised ZnPIm powder, glass and simulated patterns compared; Figure 2a corrected in 2026 correction.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Corrected powder PXRD agreement	Corrected freshly synthesised ZnPIm powder PXRD shows good agreement with the theoretical pattern.	—	—	Text Qualitative	correction p.1 · Correction · Corrected Figure 2a

Dry ZnPIm powder · Powder

Bruker D8 Advanced diffractometer with Anton Parr CHC plus non-ambient chamber; heating rate 5 C/min, isothermal scans.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Glass state after cooling	After cooling to room temperature, the MOF glass remained amorphous.	—	—	Text Qualitative	main p.2 · 2.1. Synthesis, Structure and Characterization · Figure S6
PXRD peak disappearance temperature	At 170 C the MOF powder melted and PXRD peaks disappeared.	—	—	Text Rounded Reported	main p.2 · 2.1. Synthesis, Structure and Characterization · Figure S6