Microscopy Morphology — Multi-stimulus semiconductor Cu(i)-I-pyrimidine coordination polymer with thermo- and mechanochromic sensing

Measurement evidence

Microscopy Morphology

Multi-stimulus semiconductor Cu(i)-I-pyrimidine coordination polymer with thermo- and mechanochromic sensing · Lopez J., Murillo M., Lifante-Pedrola G. et al. · CrystEngComm · 2022 · 341-349

1 measurement group · 2 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Field-emission scanning electron microscopy

Scanning electron microscopy

CP1 ground powder series · Powder

Philips XL 30 S-FEG; 300 uA electron beam; 10.0 kV; 10^-7 Pa; doped SiO2 surfaces cleaned by sonication and metallised with 10 nm Cr.

Atmosphere: High vacuum during imaging; argon drying during substrate preparation.
Geometry: Doped SiO2 substrate; 10 nm Cr coating.
Context: unground and 15 min ground pristine CP1 powder on substrate
Measurement source: main p.3 / article p.343 · Scanning electron microscopy (SEM) images · Fig. S22

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Grinding morphology change	FESEM shows unground polycrystals and 15 min ground granules/defects; grain size decreases.	—	—	Text Qualitative	main p.7 / article p.347 · Results and discussion · Fig. S22
SEM scale bars	2 um and 500 nm	—	—	Caption Rounded Reported	SI p.17 · S7 SEM Images · Fig. S22