Other — Multi-stimulus semiconductor Cu(i)-I-pyrimidine coordination polymer with thermo- and mechanochromic sensing

Measurement evidence

Other

Multi-stimulus semiconductor Cu(i)-I-pyrimidine coordination polymer with thermo- and mechanochromic sensing · Lopez J., Murillo M., Lifante-Pedrola G. et al. · CrystEngComm · 2022 · 341-349

1 measurement group · 6 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Thermogravimetric analysis coupled to differential thermal analysis (TGA-DTA)

Calorimetry and thermal analysis Thermogravimetric analysis

CP1 precipitated bulk solid / polycrystalline powder · Powder

TA Instruments Q500; nitrogen flow 90 mL min^-1; heating rate 10 C min^-1; 25 to 1000 C.

Temperature: 298 to 1273
Atmosphere: Nitrogen gas
Geometry: Pt sample holder.
Context: pristine CP1 powder
Measurement source: main p.2 / article p.342 · Materials and methods · Fig. S7; Table S4

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
CuI decomposition temperature	607 C	—	—	Text Rounded Reported	main p.4 / article p.344 · Results and discussion · Fig. S7; Table S4
Maximum derivative weight loss	0.8104 %/C	—	—	SI Table Exact Reported	SI p.8 · S3 Thermogravimetric analysis · Table S4
Residual weight	16.17%	—	—	SI Table Exact Reported	SI p.8 · S3 Thermogravimetric analysis · Table S4
Second TGA mass-loss event	535 C, loss of remaining ligand	—	—	Text Rounded Reported	main p.4 / article p.344 · Results and discussion · Fig. S7; Table S4
T5% decomposition temperature	174 C	—	—	SI Table Exact Reported	SI p.8 · S3 Thermogravimetric analysis · Table S4
Maximum decomposition-rate temperature	182 C	—	—	SI Table Exact Reported	SI p.8 · S3 Thermogravimetric analysis · Table S4