Porosity — Nanosheets of Two-Dimensional Magnetic and Conducting Fe(II)/Fe(III) Mixed-Valence Metal-Organic Frameworks

2 measurement groups · 2 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

compound 1 THF-exchanged and evacuated powder · Powder

Water in channels partially exchanged with THF; sample evacuated at 100 C; PXRD compared with pristine pattern.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
PXRD after THF exchange and evacuation	PXRD patterns after THF exchange and evacuation are very similar, indicating general structure is kept; solvent removal incomplete at 100 C	—	—	Qualitative Qualitative	S-12-S-13 · Water removal · Figure S16

compound 2 THF-exchanged and evacuated powder · Powder

Water in channels partially exchanged with THF; sample evacuated at 100 C; PXRD compared with pristine pattern.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
PXRD after THF exchange and evacuation	PXRD patterns after THF exchange and evacuation are very similar, indicating general structure is kept; solvent removal incomplete at 100 C	—	—	Qualitative Qualitative	S-12-S-13 · Water removal · Figure S17