Diffraction Structure — Electrically Conductive Metal–Organic Framework Thin Film-Based On-Chip Micro-Biosensor: A Platform to Unravel Surface Morphology-Dependent Biosensing

Measurement evidence

Diffraction Structure

Electrically Conductive Metal–Organic Framework Thin Film-Based On-Chip Micro-Biosensor: A Platform to Unravel Surface Morphology-Dependent Biosensing · Chen X., Dong J., Chi K. et al. · Advanced Functional Materials · 2021 · 2102855

2 measurement groups · 11 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

2D grazing-incidence wide-angle X-ray scattering (GIWAXS)

Pristine Cu-BHT thin film · Thin Film

Synchrotron GIWAXS used to determine crystallographic reflection centres, interlayer distance, and face-on orientation.

Context
pristine Cu-BHT film
Measurement source
p003 · Results and Discussion · Figure 2d-f
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Edge-on crystallite orientation fraction1.8% edge-onText
Exact Reported
p004 · Results and Discussion · Figure 2f
Face-on crystallite orientation fractionMarked as a best value within this paper98.2% face-on; edge-on/face-on area ratio about 1:49Text
Exact Reported
p004 · Results and Discussion · Figure 2f
GIWAXS interlayer distance3.23 AText
Exact Reported
p003 · Results and Discussion · Figure 2d
GIWAXS qz reflection assigned to (001)qz = 1.94 A-1Text
Rounded Reported
p003 · Results and Discussion · Figure 2d
GIWAXS qz reflection assigned to (010)qz = 0.63 A-1Text
Rounded Reported
p003 · Results and Discussion · Figure 2d
GIWAXS qz reflection assigned to (100)qz = 0.60 A-1Text
Rounded Reported
p003 · Results and Discussion · Figure 2d
GIWAXS qz reflection assigned to (110)qz = 0.96 A-1Text
Rounded Reported
p003 · Results and Discussion · Figure 2d
GIWAXS qz reflection assigned to (200)qz = 0.92 A-1Text
Rounded Reported
p003 · Results and Discussion · Figure 2d

Powder X-ray diffraction with Pawley refinement

Pristine Cu-BHT thin film · Thin Film

PXRD pattern reproduced using eclipsed AA stacking model; Bruker D8 Advance with Cu Kalpha source in theta/2theta Bragg-Brentano geometry.

Atmosphere
ambient
Context
pristine Cu-BHT film
Measurement source
p003 · Results and Discussion · Figure 2a / Figures S4-S5
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
PXRD-refined lattice parameter aa = 8.22 AText
Rounded Reported
p003 · Results and Discussion · Figure 2a
PXRD-refined lattice parameter bb = 8.59 AText
Rounded Reported
p003 · Results and Discussion · Figure 2a
PXRD-refined lattice parameter cc = 3.17 AText
Rounded Reported
p003 · Results and Discussion · Figure 2a / Figure S5