Spectroscopy — Electrically Conductive Metal–Organic Framework Thin Film-Based On-Chip Micro-Biosensor: A Platform to Unravel Surface Morphology-Dependent Biosensing

Measurement evidence

Spectroscopy

Electrically Conductive Metal–Organic Framework Thin Film-Based On-Chip Micro-Biosensor: A Platform to Unravel Surface Morphology-Dependent Biosensing · Chen X., Dong J., Chi K. et al. · Advanced Functional Materials · 2021 · 2102855

3 measurement groups · 10 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

FT-IR spectroscopy

Pristine Cu-BHT thin film · Thin Film

FT-IR spectra in 4000-400 cm-1 region using KBr pellets compared ligand and Cu-BHT film.

Context
pristine Cu-BHT film
Measurement source
p003 · Results and Discussion · Figure S3
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Absence of residual thiol S-H peakno -SH peak at 2490 cm-1Text
Qualitative
p003 · Results and Discussion · Figure S3

UV-vis transmittance spectroscopy

Cu-BHT film on quartz wafer · Thin Film

Cu-BHT thin film transferred to quartz wafer; transmittance spectrum recorded from visible to near-infrared range.

Geometry
film on quartz wafer
Context
pristine Cu-BHT film
Measurement source
p005 · Supporting Information · Figure S7
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Average optical transmittanceaverage transmittance approx 83%; Figure S7 label 83.14%Figure Axis
Rounded Reported
p005 · Supporting Information · Figure S7

XPS Cu 2p and Cu LMM Auger spectroscopy

Pristine Cu-BHT thin film · Thin Film

Comparison of bottom-side and up-side surfaces to quantify s-Cu and ts-Cu defect-site percentages; C 1s set to 284.8 eV for charge correction.

Context
pristine Cu-BHT film surface comparison
Measurement source
p006-p007 · Results and Discussion · Figure 5b / Figures S19-S21
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Cu LMM s-Cu kinetic energy917.9 eVText
Exact Reported
p006 · Results and Discussion · Figure S20
Bottom-side ts-Cu percentage from Cu LMM AugerMarked as a best value within this paperts-Cu = 41.25%Text
Exact Reported
p006 · Results and Discussion · Figure S20
Cu LMM ts-Cu kinetic energy913.8 eVText
Exact Reported
p006 · Results and Discussion · Figure S20
Up-side ts-Cu percentage from Cu LMM Augerts-Cu = 27.46%Text
Exact Reported
p006 · Results and Discussion · Figure S20
Cu 2p3/2 s-Cu peak binding energynear 931.8 eVText
Approximate
p006 · Results and Discussion · Figure 5b
Bottom-side ts-Cu percentage from Cu 2p XPSMarked as a best value within this paperts-Cu = 51.32%Text
Exact Reported
p006 · Results and Discussion · Figure 5b
Cu 2p3/2 ts-Cu peak binding energynear 933.2 eVText
Approximate
p006 · Results and Discussion · Figure 5b
Up-side ts-Cu percentage from Cu 2p XPSts-Cu = 35.24%Text
Exact Reported
p006 · Results and Discussion · Figure 5b