Microscopy Morphology — Continuous and reversible tuning of inter-layer spacings in two-dimensional conductive metal organic frameworks

2 measurement groups · 2 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Heat-treated Ga9HHTP4 (HT-Ga9HHTP4) · Powder

SEM before/after heating; Zeiss Merlin high-resolution SEM with InLens detector.

Geometry: Operating voltage 1-4 kV
Context: heated sample compared with pristine morphology
Measurement source: p003 · Solvent removal/exchange in Ga9HHTP4 · Fig. 1f and Fig. S2

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Ga9HHTP4 morphology after heating	Hexagonal rod-like morphology retained; no notable changes compared with pristine.	—	—	Text Qualitative	p003 · Solvent removal/exchange in Ga9HHTP4 · Fig. 1f

Ga9HHTP4 multi-sample comparison series · Powder

Colloidal samples drop-cast on lacey carbon TEM grids and dried 24 h before imaging.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
ACN-soaked Ga9HHTP4 TEM/FFT spacing	~3.32 Angstrom from Fig. 2e inset	—	—	Figure Axis Approximate	p003 · Fig. 2 · Fig. 2e