Diffraction Structure — NH2-UiO-66 Metal-Organic Framework Nanoparticles for Hydroxide Ion Conductive Photoswitches

Measurement evidence

Diffraction Structure

NH2-UiO-66 Metal-Organic Framework Nanoparticles for Hydroxide Ion Conductive Photoswitches · Wang S., Fan S., Fang Z. et al. · ACS Applied Nano Materials · 2021 · 8352-8359

3 measurement groups · 6 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Powder X-ray diffraction before and after conductivity testing

NH2-UiO-66-10-OH · Pellet

XRD patterns of NH2-UiO-66-10 and NH2-UiO-66-50 before and after KOH/conductivity testing.

Context
KOH-treated OH-loaded samples before/after testing
Measurement source
p004 · Additional figures · Figure S3
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
framework crystallinity after KOH/conductivity testNH2-UiO-66-10-OH after test and NH2-UiO-66-50-OH after test retain XRD features; -50 remains more crystallineQualitative
Qualitative
p004 · Additional figures · Figure S3

Powder X-ray diffraction; SI modulator series comparison

NH2-UiO-66-0 · Powder

XRD patterns of NH2-UiO-66 samples prepared with 0, 10, 50, and 100 equiv acetic-acid modulator.

Context
pristine framework powders
Measurement source
p002 · Additional figures · Figure S1b
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
XRD crystallinity trend with acetic-acid modulatorcrystallinity increases from NH2-UiO-66-0/10 to NH2-UiO-66-50/100Qualitative
Qualitative
p002 · Additional figures · Figure S1b

Powder X-ray diffraction with Cu Kalpha radiation

NH2-UiO-66-50 · Powder

XRD patterns compared against simulated NH2-UiO-66.

Context
pristine framework powder
Measurement source
p002-p006 · Result and Discussion; Methods · Figure 1c
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
reported nanopore size1 nm1 nmText
Rounded Reported
p002 · Introduction
reported triangular window size0.6 nm0.6 nmText
Rounded Reported
p002 · Introduction
XRD characteristic peak7.36 deg 2theta7.36 deg 2thetaText
Exact Reported
p002 · Result and Discussion · Figure 1c
XRD characteristic peak8.48 deg 2theta8.48 deg 2thetaText
Exact Reported
p002 · Result and Discussion · Figure 1c