Other — Ligand-Insertion Strategy for Constructing 2D Conjugated Metal–Organic Framework with Large Pore Size for Electrochemical Analytics

Measurement evidence

Other

Ligand-Insertion Strategy for Constructing 2D Conjugated Metal–Organic Framework with Large Pore Size for Electrochemical Analytics · Wang X.-Z., Chen Y., Cao X.-M. et al. · Angewandte Chemie - International Edition · 2025 · e202413115

1 measurement group · 4 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Thermogravimetric analysis, solvent-immersion PXRD, salt-immersion PXRD/EDS and zeta potential

X-ray diffraction and scattering Dynamic light scattering and zeta potential Elemental microanalysis and mapping Thermogravimetric analysis

As-prepared Cu3(HHTP)(DHBQ)1.5/1.53 black powder · Powder

TG in N2 from ambient to 700 deg C at 10 deg C min-1; solvent immersion for 3 days; saturated NaCl/KCl overnight; zeta potential in ultrasonicated deionized-water suspension.

Atmosphere: N2 for TGA; aqueous suspension for zeta potential
Geometry: powder dispersion/suspension
Context: pristine_framework
Measurement source: 4 · Structural Characterization on the Sample · Figures S8-S13

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Fraction of H2en2+ replaced by K+	38%	—	—	Caption Exact Reported	7 · Figure S9 · Figure S9
Fraction of H2en2+ replaced by Na+	26%	—	—	Caption Exact Reported	7 · Figure S9 · Figure S9
Thermal stability below temperature	stable below 250 deg C	523.15 K	—	Text Rounded Reported	4 · Structural Characterization on the Sample · Figure S11
Zeta potential in water suspension	-13.20 mV	—	—	Text Exact Reported	4 · Structural Characterization on the Sample · Figure S13