Spectroscopy — High-κ Samarium-Based Metal-Organic Framework for Gate Dielectric Applications

Measurement evidence

Spectroscopy

High-κ Samarium-Based Metal-Organic Framework for Gate Dielectric Applications · Pathak A., Chiou G.R., Gade N.R. et al. · ACS Applied Materials and Interfaces · 2017 · 21872-21878

1 measurement group · 4 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

FTIR in KBr pellets and CHN elemental analysis

as-synthesised compound 1 crystals · Single Crystal

FTIR 4000-400 cm-1 on Perkin-Elmer Paragon 1000; elemental analysis on Perkin-Elmer 2400 CHN analyser.

Geometry
KBr pellet for FTIR
Context
pristine framework
Measurement source
p002 / journal page 21873 · 2.1-2.2 · Figure S1
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
elemental analysis carbon foundcalcd C 19.35%; found C 19.33%Text
Exact Reported
p002 / journal page 21873 · 2.2. Synthesis
elemental analysis hydrogen foundcalcd H 1.62%; found H 1.60%Text
Exact Reported
p002 / journal page 21873 · 2.2. Synthesis
representative FTIR band1602(m) cm-1 for compound 1Text
Exact Reported
p002 / journal page 21873 · 2.2. Synthesis · Figure S1
isolated yield of compound 155.1% (41.8 mg; 0.05 mmol)Text
Exact Reported
p002 / journal page 21873 · 2.2. Synthesis