Other — Enhancing Proton Conductivity and Dimensional Stability of Nanofiber Proton Exchange Membranes through In Situ Growth of MOF-Modified PVDF Nanofibers

Measurement evidence

Other

Enhancing Proton Conductivity and Dimensional Stability of Nanofiber Proton Exchange Membranes through In Situ Growth of MOF-Modified PVDF Nanofibers · Sun J., Han D., Dong R. et al. · Energy and Fuels · 2024 · 7322-7330

13 measurement groups · 45 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

tensile testing

A-PVDF-N@Nafion · Thin Film

5 x 1 cm strips; stretching speed 4 mm/min; average of 2-3 measurements

Geometry
mechanical strip test
Context
PEM mechanical property
Measurement source
p003 / journal page 7324 · 2.3 Characterization · Table 1
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
elongation at break12.13%——Table
Exact Reported
p007 / journal page 7328 · 3.2 Characterization of PVDF/UIO@Nafion · Table 1
tensile strength14.8 MPa——Table
Exact Reported
p007 / journal page 7328 · 3.2 Characterization of PVDF/UIO@Nafion · Table 1

tensile testing

A-PVDF@Nafion · Thin Film

5 x 1 cm strips; stretching speed 4 mm/min; average of 2-3 measurements

Geometry
mechanical strip test
Context
PEM mechanical property
Measurement source
p003 / journal page 7324 · 2.3 Characterization · Table 1
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
elongation at break21.1%——Table
Exact Reported
p007 / journal page 7328 · 3.2 Characterization of PVDF/UIO@Nafion · Table 1
tensile strength18.69 MPa——Table
Exact Reported
p007 / journal page 7328 · 3.2 Characterization of PVDF/UIO@Nafion · Table 1

tensile testing

A-PVDF-NS@Nafion · Thin Film

5 x 1 cm strips; stretching speed 4 mm/min; average of 2-3 measurements

Geometry
mechanical strip test
Context
PEM mechanical property
Measurement source
p003 / journal page 7324 · 2.3 Characterization · Table 1
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
elongation at break34.76%——Table
Exact Reported
p007 / journal page 7328 · 3.2 Characterization of PVDF/UIO@Nafion · Table 1
tensile strength12.12 MPa——Table
Exact Reported
p007 / journal page 7328 · 3.2 Characterization of PVDF/UIO@Nafion · Table 1

tensile testing

Nafion · Thin Film

5 x 1 cm strips; stretching speed 4 mm/min; average of 2-3 measurements

Geometry
mechanical strip test
Context
PEM mechanical property
Measurement source
p003 / journal page 7324 · 2.3 Characterization · Table 1
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
elongation at break117.67%——Table
Exact Reported
p007 / journal page 7328 · 3.2 Characterization of PVDF/UIO@Nafion · Table 1
tensile strength11.21 MPa——Table
Exact Reported
p007 / journal page 7328 · 3.2 Characterization of PVDF/UIO@Nafion · Table 1

tensile testing

PVDF@Nafion · Thin Film

5 x 1 cm strips; stretching speed 4 mm/min; average of 2-3 measurements

Geometry
mechanical strip test
Context
PEM mechanical property
Measurement source
p003 / journal page 7324 · 2.3 Characterization · Table 1
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
elongation at break107.17%——Table
Exact Reported
p007 / journal page 7328 · 3.2 Characterization of PVDF/UIO@Nafion · Table 1
tensile strength16.55 MPa——Table
Exact Reported
p007 / journal page 7328 · 3.2 Characterization of PVDF/UIO@Nafion · Table 1

TGA (Netzsch STA 449 F3)

A-PVDF-N@Nafion · Thin Film

30-800 C at 10 C/min in N2

Atmosphere
N2
Geometry
thermogravimetric heating
Context
PEM thermal stability
Measurement source
p003 / journal page 7324 · 2.3 Characterization · Figure 7
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
thermal stability versus Nafionhigher thermal decomposition temperature and reduced mass loss relative to Nafion——Text
Qualitative
p007 / journal page 7328 · 3.2 Characterization of PVDF/UIO@Nafion · Figure 7

TGA (Netzsch STA 449 F3)

A-PVDF-NS@Nafion · Thin Film

30-800 C at 10 C/min in N2

Atmosphere
N2
Geometry
thermogravimetric heating
Context
PEM thermal stability
Measurement source
p003 / journal page 7324 · 2.3 Characterization · Figure 7
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
thermal stability versus Nafionhigher thermal decomposition temperature and reduced mass loss relative to Nafion——Text
Qualitative
p007 / journal page 7328 · 3.2 Characterization of PVDF/UIO@Nafion · Figure 7

TGA (Netzsch STA 449 F3)

Nafion · Thin Film

30-800 C at 10 C/min in N2

Atmosphere
N2
Geometry
thermogravimetric heating
Context
PEM thermal stability
Measurement source
p003 / journal page 7324 · 2.3 Characterization · Figure 7
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Nafion/composite TGA degradation ranges110-250 C bound water/solvent; 250-400 C SO3H to SO2/SO3; above 400 C polymer backbone——Text
Range
p007 / journal page 7328 · 3.2 Characterization of PVDF/UIO@Nafion · Figure 7

water uptake and swelling ratio gravimetry/area measurement

A-PVDF-N@Nafion · Thin Film

3 x 1 cm strips dried at 60 C for 8 h, immersed in deionised water at 40, 60, 80 C for 12 h

Atmosphere
deionised water
Geometry
mass and area change, equations 3 and 4
Context
water uptake/swelling context for PEM dimensional stability
Measurement source
p003 / journal page 7324 · 2.3 Characterization · Figure 6
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
swelling ratio at 40 Capproximately 3.9%——Figure Axis
Approximate
p006 / journal page 7327 · 3.2 Characterization of PVDF/UIO@Nafion · Figure 6b
swelling ratio at 60 Capproximately 6.7%——Figure Axis
Approximate
p006 / journal page 7327 · 3.2 Characterization of PVDF/UIO@Nafion · Figure 6b
swelling ratio at 80 Capproximately 8.7%——Figure Axis
Approximate
p006 / journal page 7327 · 3.2 Characterization of PVDF/UIO@Nafion · Figure 6b
maximum swelling ratio reduction versus Nafion59.16%——Text
Exact Reported
p006 / journal page 7327 · 3.2 Characterization of PVDF/UIO@Nafion · Figure 6b
water uptake at 40 Capproximately 16.5%——Figure Axis
Approximate
p006 / journal page 7327 · 3.2 Characterization of PVDF/UIO@Nafion · Figure 6a
water uptake at 60 Capproximately 22.0%——Figure Axis
Approximate
p006 / journal page 7327 · 3.2 Characterization of PVDF/UIO@Nafion · Figure 6a
water uptake at 80 Capproximately 33.0%——Figure Axis
Approximate
p006 / journal page 7327 · 3.2 Characterization of PVDF/UIO@Nafion · Figure 6a

water uptake and swelling ratio gravimetry/area measurement

A-PVDF@Nafion · Thin Film

3 x 1 cm strips dried at 60 C for 8 h, immersed in deionised water at 40, 60, 80 C for 12 h

Atmosphere
deionised water
Geometry
mass and area change, equations 3 and 4
Context
water uptake/swelling context for PEM dimensional stability
Measurement source
p003 / journal page 7324 · 2.3 Characterization · Figure 6
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
swelling ratio at 40 Capproximately 2.3%——Figure Axis
Approximate
p006 / journal page 7327 · 3.2 Characterization of PVDF/UIO@Nafion · Figure 6b
swelling ratio at 60 Capproximately 5.1%——Figure Axis
Approximate
p006 / journal page 7327 · 3.2 Characterization of PVDF/UIO@Nafion · Figure 6b
swelling ratio at 80 Capproximately 6.4%——Figure Axis
Approximate
p006 / journal page 7327 · 3.2 Characterization of PVDF/UIO@Nafion · Figure 6b
water uptake at 40 Capproximately 14.0%——Figure Axis
Approximate
p006 / journal page 7327 · 3.2 Characterization of PVDF/UIO@Nafion · Figure 6a
water uptake at 60 Capproximately 21.0%——Figure Axis
Approximate
p006 / journal page 7327 · 3.2 Characterization of PVDF/UIO@Nafion · Figure 6a
water uptake at 80 Capproximately 28.0%——Figure Axis
Approximate
p006 / journal page 7327 · 3.2 Characterization of PVDF/UIO@Nafion · Figure 6a

water uptake and swelling ratio gravimetry/area measurement

A-PVDF-NS@Nafion · Thin Film

3 x 1 cm strips dried at 60 C for 8 h, immersed in deionised water at 40, 60, 80 C for 12 h

Atmosphere
deionised water
Geometry
mass and area change, equations 3 and 4
Context
water uptake/swelling context for PEM dimensional stability
Measurement source
p003 / journal page 7324 · 2.3 Characterization · Figure 6
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
swelling ratio at 40 Capproximately 4.0%——Figure Axis
Approximate
p006 / journal page 7327 · 3.2 Characterization of PVDF/UIO@Nafion · Figure 6b
swelling ratio at 60 Capproximately 6.8%——Figure Axis
Approximate
p006 / journal page 7327 · 3.2 Characterization of PVDF/UIO@Nafion · Figure 6b
swelling ratio at 80 Capproximately 12.7%——Figure Axis
Approximate
p006 / journal page 7327 · 3.2 Characterization of PVDF/UIO@Nafion · Figure 6b
maximum swelling ratio reduction versus Nafion57.94%——Text
Exact Reported
p006 / journal page 7327 · 3.2 Characterization of PVDF/UIO@Nafion · Figure 6b
water uptake at 40 Capproximately 21.0%——Figure Axis
Approximate
p006 / journal page 7327 · 3.2 Characterization of PVDF/UIO@Nafion · Figure 6a
water uptake at 60 Capproximately 26.5%——Figure Axis
Approximate
p006 / journal page 7327 · 3.2 Characterization of PVDF/UIO@Nafion · Figure 6a
water uptake at 80 Capproximately 36.0%——Figure Axis
Approximate
p006 / journal page 7327 · 3.2 Characterization of PVDF/UIO@Nafion · Figure 6a

water uptake and swelling ratio gravimetry/area measurement

Nafion · Thin Film

3 x 1 cm strips dried at 60 C for 8 h, immersed in deionised water at 40, 60, 80 C for 12 h

Atmosphere
deionised water
Geometry
mass and area change, equations 3 and 4
Context
water uptake/swelling context for PEM dimensional stability
Measurement source
p003 / journal page 7324 · 2.3 Characterization · Figure 6
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
swelling ratio at 40 Capproximately 9.8%——Figure Axis
Approximate
p006 / journal page 7327 · 3.2 Characterization of PVDF/UIO@Nafion · Figure 6b
swelling ratio at 60 Capproximately 11.3%——Figure Axis
Approximate
p006 / journal page 7327 · 3.2 Characterization of PVDF/UIO@Nafion · Figure 6b
swelling ratio at 80 Capproximately 12.7%——Figure Axis
Approximate
p006 / journal page 7327 · 3.2 Characterization of PVDF/UIO@Nafion · Figure 6b
water uptake at 40 Capproximately 27.0%——Figure Axis
Approximate
p006 / journal page 7327 · 3.2 Characterization of PVDF/UIO@Nafion · Figure 6a
water uptake at 60 Capproximately 30.5%——Figure Axis
Approximate
p006 / journal page 7327 · 3.2 Characterization of PVDF/UIO@Nafion · Figure 6a
water uptake at 80 Capproximately 38.0%——Figure Axis
Approximate
p006 / journal page 7327 · 3.2 Characterization of PVDF/UIO@Nafion · Figure 6a

water uptake and swelling ratio gravimetry/area measurement

PVDF@Nafion · Thin Film

3 x 1 cm strips dried at 60 C for 8 h, immersed in deionised water at 40, 60, 80 C for 12 h

Atmosphere
deionised water
Geometry
mass and area change, equations 3 and 4
Context
water uptake/swelling context for PEM dimensional stability
Measurement source
p003 / journal page 7324 · 2.3 Characterization · Figure 6
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
swelling ratio at 40 Capproximately 1.5%——Figure Axis
Approximate
p006 / journal page 7327 · 3.2 Characterization of PVDF/UIO@Nafion · Figure 6b
swelling ratio at 60 Capproximately 2.6%——Figure Axis
Approximate
p006 / journal page 7327 · 3.2 Characterization of PVDF/UIO@Nafion · Figure 6b
swelling ratio at 80 Capproximately 4.6%——Figure Axis
Approximate
p006 / journal page 7327 · 3.2 Characterization of PVDF/UIO@Nafion · Figure 6b
water uptake at 40 Capproximately 11.0%——Figure Axis
Approximate
p006 / journal page 7327 · 3.2 Characterization of PVDF/UIO@Nafion · Figure 6a
water uptake at 60 Capproximately 19.0%——Figure Axis
Approximate
p006 / journal page 7327 · 3.2 Characterization of PVDF/UIO@Nafion · Figure 6a
water uptake at 80 Capproximately 25.0%——Figure Axis
Approximate
p006 / journal page 7327 · 3.2 Characterization of PVDF/UIO@Nafion · Figure 6a