Diffraction Structure — Structure and Electrical Transport Properties of Metal Cate-Cholate Frameworks: The Metal Center Matters†

6 measurement groups · 6 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Ca-HHTP powder sample · Powder

Rigaku sixth-generation MiniFlex; Cu Kalpha radiation, 600 W (40 kV, 15 mA); powder sample.

Context: pristine powder
Measurement source: SI p.S3 and S10 · Materials and Methods; Powder X-ray Diffraction · Figure 1a; Figure S5/S6

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Ca-HHTP Pawley a=b	a = b = 22.2 A	—	—	Text Exact Reported	main p.2, article p.312 · Preparation and structural characterizations · Figure S5
Ca-HHTP Pawley c	c = 13.3 A	—	—	Text Exact Reported	main p.2, article p.312 · Preparation and structural characterizations · Figure S5
Ca-HHTP Pawley final Rwp	Rwp = 5.47%	—	—	Text Exact Reported	main p.2, article p.312 · Preparation and structural characterizations · Figure S5

Co-HHTP powder sample · Powder

Rigaku sixth-generation MiniFlex; Cu Kalpha radiation, 600 W (40 kV, 15 mA); powder sample.

Context: pristine powder
Measurement source: SI p.S3 and S10 · Materials and Methods; Powder X-ray Diffraction · Figure 1a; Figure S5/S6

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source

Cu-HHTP powder sample · Powder

Rigaku sixth-generation MiniFlex; Cu Kalpha radiation, 600 W (40 kV, 15 mA); powder sample.

Context: pristine powder
Measurement source: SI p.S3 and S10 · Materials and Methods; Powder X-ray Diffraction · Figure 1a; Figure S5/S6

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source

Mg-HHTP powder sample · Powder

Rigaku sixth-generation MiniFlex; Cu Kalpha radiation, 600 W (40 kV, 15 mA); powder sample.

Context: pristine powder
Measurement source: SI p.S3 and S10 · Materials and Methods; Powder X-ray Diffraction · Figure 1a; Figure S5/S6

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Common PXRD 100 reflection	4.8 deg 2theta	—	—	Text Rounded Reported	main p.2-p.3, article p.312-p.313 · Preparation and structural characterizations · Figure 1; Figure S8
Common PXRD 200 reflection	9.6 deg 2theta	—	—	Text Rounded Reported	main p.2-p.3, article p.312-p.313 · Preparation and structural characterizations · Figure 1; Figure S8
Common PXRD 210 reflection	13.9 deg 2theta	—	—	Text Rounded Reported	main p.2-p.3, article p.312-p.313 · Preparation and structural characterizations · Figure 1; Figure S8

Ni-HHTP powder sample · Powder

Rigaku sixth-generation MiniFlex; Cu Kalpha radiation, 600 W (40 kV, 15 mA); powder sample.

Context: pristine powder
Measurement source: SI p.S3 and S10 · Materials and Methods; Powder X-ray Diffraction · Figure 1a; Figure S5/S6

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source

Zn-HHTP powder sample · Powder

Rigaku sixth-generation MiniFlex; Cu Kalpha radiation, 600 W (40 kV, 15 mA); powder sample.

Context: pristine powder
Measurement source: SI p.S3 and S10 · Materials and Methods; Powder X-ray Diffraction · Figure 1a; Figure S5/S6

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source