Microscopy Morphology — Structure and Electrical Transport Properties of Metal Cate-Cholate Frameworks: The Metal Center Matters†

Measurement evidence

Microscopy Morphology

Structure and Electrical Transport Properties of Metal Cate-Cholate Frameworks: The Metal Center Matters† · Yang M., Zhu R., Chen X. et al. · Chinese Journal of Chemistry · 2026 · 311-318

18 measurement groups · 13 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Atomic force microscopy (AFM) thickness

Ca-HHTP film sample · Thin Film

Tapping-mode AFM on M-HHTP film on quartz glass substrate.

Geometry
film on quartz glass substrate
Context
pristine film
Measurement source
SI p.S17 · Atomic Force Microscope · Figure S14
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Ca-HHTP film thickness by AFM500 nm500 nmVisual Estimate
Approximate
SI p.S17 · Atomic Force Microscope · Figure S14

HRTEM with FFT

Ca-HHTP powder sample · Powder

JEM-2100 Plus, 200 kV; powders dispersed in ethanol, drop-cast on carbon-coated copper grid and dried ambient.

Atmosphere
ambient drying after grid preparation
Geometry
carbon-coated copper grid
Context
pristine powder
Measurement source
SI p.S12 · Transmission Electron Microscopy · Figure S8
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource

Scanning electron microscopy (SEM)

Ca-HHTP powder sample · Powder

Quanta FEG 250; 7 mm working distance, 10 kV beamline, 10^-6 torr chamber; sample on carbon conductive tape/aluminum plate.

Atmosphere
10^-6 torr vacuum chamber
Context
pristine powder
Measurement source
SI p.S11 · Scanning Electron Microscopy · Figure S7
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Ca-HHTP SEM morphologyrod-like morphology; well-formed single crystals exceeding 20 um in lengthText
Qualitative
main p.3, article p.313 · Preparation and structural characterizations · Figure 2; Figure S7

Atomic force microscopy (AFM) thickness

Co-HHTP film sample · Thin Film

Tapping-mode AFM on M-HHTP film on quartz glass substrate.

Geometry
film on quartz glass substrate
Context
pristine film
Measurement source
SI p.S17 · Atomic Force Microscope · Figure S14
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Co-HHTP film thickness by AFM300 nm300 nmVisual Estimate
Approximate
SI p.S17 · Atomic Force Microscope · Figure S14

HRTEM with FFT

Co-HHTP powder sample · Powder

JEM-2100 Plus, 200 kV; powders dispersed in ethanol, drop-cast on carbon-coated copper grid and dried ambient.

Atmosphere
ambient drying after grid preparation
Geometry
carbon-coated copper grid
Context
pristine powder
Measurement source
SI p.S12 · Transmission Electron Microscopy · Figure S8
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource

Scanning electron microscopy (SEM)

Co-HHTP powder sample · Powder

Quanta FEG 250; 7 mm working distance, 10 kV beamline, 10^-6 torr chamber; sample on carbon conductive tape/aluminum plate.

Atmosphere
10^-6 torr vacuum chamber
Context
pristine powder
Measurement source
SI p.S11 · Scanning Electron Microscopy · Figure S7
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Co-HHTP SEM morphologyrod-like morphology; well-formed single crystals exceeding 20 um in lengthText
Qualitative
main p.3, article p.313 · Preparation and structural characterizations · Figure 2; Figure S7

Atomic force microscopy (AFM) thickness

Cu-HHTP film sample · Thin Film

Tapping-mode AFM on M-HHTP film on quartz glass substrate.

Geometry
film on quartz glass substrate
Context
pristine film
Measurement source
SI p.S17 · Atomic Force Microscope · Figure S14
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Cu-HHTP film thickness by AFM500 nm500 nmVisual Estimate
Approximate
SI p.S17 · Atomic Force Microscope · Figure S14

HRTEM with FFT

Cu-HHTP powder sample · Powder

JEM-2100 Plus, 200 kV; powders dispersed in ethanol, drop-cast on carbon-coated copper grid and dried ambient.

Atmosphere
ambient drying after grid preparation
Geometry
carbon-coated copper grid
Context
pristine powder
Measurement source
SI p.S12 · Transmission Electron Microscopy · Figure S8
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource

Scanning electron microscopy (SEM)

Cu-HHTP powder sample · Powder

Quanta FEG 250; 7 mm working distance, 10 kV beamline, 10^-6 torr chamber; sample on carbon conductive tape/aluminum plate.

Atmosphere
10^-6 torr vacuum chamber
Context
pristine powder
Measurement source
SI p.S11 · Scanning Electron Microscopy · Figure S7
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Cu-HHTP SEM morphologyrod-like morphology; well-formed single crystals exceeding 20 um in lengthText
Qualitative
main p.3, article p.313 · Preparation and structural characterizations · Figure 2; Figure S7

Atomic force microscopy (AFM) thickness

Mg-HHTP film sample · Thin Film

Tapping-mode AFM on M-HHTP film on quartz glass substrate.

Geometry
film on quartz glass substrate
Context
pristine film
Measurement source
SI p.S17 · Atomic Force Microscope · Figure S14
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Mg-HHTP film thickness by AFM3500 nm3500 nmVisual Estimate
Approximate
SI p.S17 · Atomic Force Microscope · Figure S14

HRTEM with FFT

Mg-HHTP powder sample · Powder

JEM-2100 Plus, 200 kV; powders dispersed in ethanol, drop-cast on carbon-coated copper grid and dried ambient.

Atmosphere
ambient drying after grid preparation
Geometry
carbon-coated copper grid
Context
pristine powder
Measurement source
SI p.S12 · Transmission Electron Microscopy · Figure S8
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
HRTEM/FFT periodicity of (100) plane1.8 nmText
Rounded Reported
main p.2-p.3, article p.312-p.313 · Preparation and structural characterizations · Figure 1; Figure S8

Scanning electron microscopy (SEM)

Mg-HHTP powder sample · Powder

Quanta FEG 250; 7 mm working distance, 10 kV beamline, 10^-6 torr chamber; sample on carbon conductive tape/aluminum plate.

Atmosphere
10^-6 torr vacuum chamber
Context
pristine powder
Measurement source
SI p.S11 · Scanning Electron Microscopy · Figure S7
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Mg-HHTP SEM morphologyrod-like morphology; well-formed single crystals exceeding 20 um in lengthText
Qualitative
main p.3, article p.313 · Preparation and structural characterizations · Figure 2; Figure S7

Atomic force microscopy (AFM) thickness

Ni-HHTP film sample · Thin Film

Tapping-mode AFM on M-HHTP film on quartz glass substrate.

Geometry
film on quartz glass substrate
Context
pristine film
Measurement source
SI p.S17 · Atomic Force Microscope · Figure S14
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Ni-HHTP film thickness by AFM150 nm150 nmVisual Estimate
Approximate
SI p.S17 · Atomic Force Microscope · Figure S14

HRTEM with FFT

Ni-HHTP powder sample · Powder

JEM-2100 Plus, 200 kV; powders dispersed in ethanol, drop-cast on carbon-coated copper grid and dried ambient.

Atmosphere
ambient drying after grid preparation
Geometry
carbon-coated copper grid
Context
pristine powder
Measurement source
SI p.S12 · Transmission Electron Microscopy · Figure S8
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource

Scanning electron microscopy (SEM)

Ni-HHTP powder sample · Powder

Quanta FEG 250; 7 mm working distance, 10 kV beamline, 10^-6 torr chamber; sample on carbon conductive tape/aluminum plate.

Atmosphere
10^-6 torr vacuum chamber
Context
pristine powder
Measurement source
SI p.S11 · Scanning Electron Microscopy · Figure S7
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Ni-HHTP SEM morphologyrod-like morphology; notably smaller grain sizesText
Qualitative
main p.3, article p.313 · Preparation and structural characterizations · Figure 2; Figure S7

Atomic force microscopy (AFM) thickness

Zn-HHTP film sample · Thin Film

Tapping-mode AFM on M-HHTP film on quartz glass substrate.

Geometry
film on quartz glass substrate
Context
pristine film
Measurement source
SI p.S17 · Atomic Force Microscope · Figure S14
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Zn-HHTP film thickness by AFM500 nm500 nmVisual Estimate
Approximate
SI p.S17 · Atomic Force Microscope · Figure S14

HRTEM with FFT

Zn-HHTP powder sample · Powder

JEM-2100 Plus, 200 kV; powders dispersed in ethanol, drop-cast on carbon-coated copper grid and dried ambient.

Atmosphere
ambient drying after grid preparation
Geometry
carbon-coated copper grid
Context
pristine powder
Measurement source
SI p.S12 · Transmission Electron Microscopy · Figure S8
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource

Scanning electron microscopy (SEM)

Zn-HHTP powder sample · Powder

Quanta FEG 250; 7 mm working distance, 10 kV beamline, 10^-6 torr chamber; sample on carbon conductive tape/aluminum plate.

Atmosphere
10^-6 torr vacuum chamber
Context
pristine powder
Measurement source
SI p.S11 · Scanning Electron Microscopy · Figure S7
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Zn-HHTP SEM morphologyrod-like morphology; notably smaller grain sizesText
Qualitative
main p.3, article p.313 · Preparation and structural characterizations · Figure 2; Figure S7