Diffraction Structure — Cooperative Proton and Li-ion Conduction in a 2D-Layered MOF via Mechanical Insertion of Lithium Halides

4 measurement groups · 5 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Ti-dobdc pristine · Pellet

Powder X-ray diffraction patterns collected for pristine Ti-dobdc and LiX-loaded samples.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
hexagonal pore diameter along c axis	7 A	—	—	Text Rounded Reported	2 · Results · Figure 1

Ti-dobdc-LiBr (MOF:LiBr = 1:1) · Pellet

Powder X-ray diffraction patterns collected for pristine Ti-dobdc and LiX-loaded samples.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
PXRD lattice expansion after LiBr insertion	anisotropic peak shift to lower angle; expanded lattice	—	—	Text Qualitative	2 · Results · Figure S2

Ti-dobdc-LiCl (MOF:LiCl = 1:1) · Pellet

Powder X-ray diffraction patterns collected for pristine Ti-dobdc and LiX-loaded samples.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
1:1 LiX sample PXRD resembles pristine Ti-dobdc	1:1 molar ratio sample exhibited a similar PXRD pattern to pristine Ti-dobdc	—	—	Text Qualitative	2 · Results · Figure 1
PXRD lattice expansion after LiCl insertion	anisotropic peak shift to lower angle; expanded lattice	—	—	Text Qualitative	2 · Results · Figure S2

Ti-dobdc-LiI (MOF:LiI = 1:1) · Pellet

Powder X-ray diffraction patterns collected for pristine Ti-dobdc and LiX-loaded samples.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
PXRD lattice expansion after LiI insertion	anisotropic peak shift to lower angle; expanded lattice	—	—	Text Qualitative	2 · Results · Figure S2