Microscopy Morphology — Aptasensor based on gold nanostructure-decorated 2D Cu metal–organic framework nanosheets for highly sensitive and specific electrochemical lipopolysaccharide detection

4 measurement groups · 10 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Au/Cu-THQ/GCE · Electrode

SEM of Au/Cu-THQ/GCE and Au/Cu-TCPP/GCE at 3.0 kV after electrode surface modification; EDS mapping in SI.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Au mass-normalised percentage on Au/Cu-TCPP/GCE surface	89.58 mass norm%	—	—	SI Table Exact Reported	12 · Supplementary Materials · Figure S8
Au atom percentage on Au/Cu-TCPP/GCE surface	48.26 atom% (main text calls this mass percentage; SI table labels it Atom [%])	—	—	SI Table Exact Reported	12 · Supplementary Materials · Figure S8
Au morphology on Cu-TCPP/GCE	AuNPs unevenly deposited on Cu-TCPP/GCE	—	—	Text Qualitative	5 · Preparation and characterization of Au/2D-MOF/GCE · Figure 2B; Figure S8
Au mass-normalised percentage on Au/Cu-THQ/GCE surfaceMarked as a best value within this paper	98.62 mass norm%	—	—	SI Table Exact Reported	13 · Supplementary Materials · Figure S9
Au atom percentage on Au/Cu-THQ/GCE surfaceMarked as a best value within this paper	84.96 atom% (main text calls this mass percentage; SI table labels it Atom [%])	—	—	SI Table Exact Reported	13 · Supplementary Materials · Figure S9
Au morphology on Cu-THQ/GCEMarked as a best value within this paper	evenly deposited and fully covered; nanoflower-like 3D architecture	—	—	Text Qualitative	5 · Preparation and characterization of Au/2D-MOF/GCE · Figure 2C; Figure S9

Cu-THQ/GCE · Electrode

SEM images of bare GCE, Cu-TCPP/GCE and Cu-THQ/GCE used to compare MOF-only electrode morphology before Au deposition.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Cu-TCPP/GCE SEM morphology	folding and wrinkling morphology on GCE	—	—	Text Qualitative	6 · Preparation and characterization of Au/2D-MOF/GCE · Figure S7B
Cu-THQ/GCE SEM morphologyMarked as a best value within this paper	flatter morphology with redox ligands and denser Cu redox sites	—	—	Text Qualitative	6 · Preparation and characterization of Au/2D-MOF/GCE · Figure S7C

Cu-TCPP nanosheets · Nanosheet

JEM 1400 TEM at 200 kV after dropping ethanolic suspension onto holey carbon-coated copper grids.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Cu-TCPP nanosheet morphology	2D nanosheet morphology with crumpled and wrinkled surfaces	—	—	Text Qualitative	4 · Characterization of the synthesized 2D Cu-MOF nanosheets · Figure 1A

Cu-THQ nanosheets · Nanosheet

JEM 1400 TEM at 200 kV after dropping ethanolic suspension onto holey carbon-coated copper grids.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Cu-THQ nanosheet morphologyMarked as a best value within this paper	2D nanosheet morphology; flatter morphology with redox ligands and denser Cu redox sites	—	—	Text Qualitative	6 · Preparation and characterization of Au/2D-MOF/GCE · Figure S7C