Spectroscopy — Aptasensor based on gold nanostructure-decorated 2D Cu metal–organic framework nanosheets for highly sensitive and specific electrochemical lipopolysaccharide detection

Measurement evidence

Spectroscopy

Aptasensor based on gold nanostructure-decorated 2D Cu metal–organic framework nanosheets for highly sensitive and specific electrochemical lipopolysaccharide detection · Tong Y., Chen M., Huang X. et al. · Microchimica Acta · 2024 · 500

3 measurement groups · 11 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

XPS

Cu-TCPP nanosheets · Nanosheet

XPS used to examine surface composition and valence states of Cu-TCPP and Cu-THQ.

Context
pristine MOF nanosheets
Measurement source
4 · Characterization of the synthesized 2D Cu-MOF nanosheets · Figures S1-S2
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Cu 2p XPS region for Cu-TCPP and Cu-THQCu-TCPP and Cu-THQ exhibit two Cu2p peaks at approximately 932-934 eV and 931-933 eV, corresponding to Cu2p3/2 and Cu2p1/2Text
Range
4 · Characterization of the synthesized 2D Cu-MOF nanosheets · Figures S1-S2

XPS

Cu-TCPP nanosheets · Nanosheet

XPS survey and high-resolution O 1s, C 1s and Cu 2p spectra for pristine Cu-TCPP nanosheets; figure labels read from rendered SI.

Geometry
nanosheet sample
Context
pristine MOF nanosheets
Measurement source
5 · Supplementary Materials · Figure S1
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Cu-TCPP C 1s C=O component288.7 eVFigure Axis
Rounded Reported
5 · Supplementary Materials · Figure S1C
Cu-TCPP C 1s C-C component284.7 eVFigure Axis
Rounded Reported
5 · Supplementary Materials · Figure S1C
Cu-TCPP C 1s C-O component285.8 eVFigure Axis
Rounded Reported
5 · Supplementary Materials · Figure S1C
Cu-TCPP O 1s C=O component531.8 eVFigure Axis
Rounded Reported
5 · Supplementary Materials · Figure S1B
Cu-TCPP O 1s C-OH component533.4 eVFigure Axis
Rounded Reported
5 · Supplementary Materials · Figure S1B

XPS

Cu-THQ nanosheets · Nanosheet

XPS survey and high-resolution O 1s, C 1s and Cu 2p spectra for pristine Cu-THQ nanosheets; figure labels read from rendered SI.

Geometry
nanosheet sample
Context
pristine MOF nanosheets
Measurement source
6 · Supplementary Materials · Figure S2
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Cu-THQ C 1s C-C component284.5 eVFigure Axis
Rounded Reported
6 · Supplementary Materials · Figure S2C
Cu-THQ C 1s C-N component285.4 eVFigure Axis
Rounded Reported
6 · Supplementary Materials · Figure S2C
Cu-THQ C 1s C-O component287.3 eVFigure Axis
Rounded Reported
6 · Supplementary Materials · Figure S2C
Cu-THQ O 1s C=O component530.1 eVFigure Axis
Rounded Reported
6 · Supplementary Materials · Figure S2B
Cu-THQ O 1s C-O component531.2 eVFigure Axis
Rounded Reported
6 · Supplementary Materials · Figure S2B