Electrochemistry Application — Conductive Ni3(HITP)2 nanofilm with asymmetrical morphology prepared by gas–liquid interface self-assembly for glucose sensing

4 measurement groups · 7 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

DS-Ni-HITP-3 min/ITO electrode · Electrode

5.0 mM K3[Fe(CN)6] containing 0.1 M KCl; scan-rate dependent CV; effective catalytic activity surface area calculated from Ip-v^1/2 slope.

Temperature: 298
Geometry: three-electrode cell; Ni3(HITP)2 film/ITO working electrode, Ag/AgCl reference, Pt counter
Context: pristine Ni3(HITP)2 film on ITO electrode
Measurement source: p002 and p006 / 2376 and 2380 · Electrochemical measurements; Results and discussion · Fig. S5

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Effective catalytic activity surface area of DS-Ni-HITPMarked as a best value within this paper	0.315 cm2	—	—	Text Exact Reported	p006 / 2380 · Results and discussion · Fig. S5
Randles-Sevcik calibration slope for DS-Ni-HITP-3 min/ITOMarked as a best value within this paper	y = 0.0946x + 0.15	—	—	Visual Estimate Approximate	p004 · Supporting Information · Fig. S5c

bare ITO · Electrode

5.0 mM K3[Fe(CN)6] containing 0.1 M KCl; scan-rate dependent CV.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Effective catalytic activity surface area of bare ITO	0.129 cm2	—	—	Text Exact Reported	p006 / 2380 · Results and discussion · Fig. S5
Randles-Sevcik calibration slope for bare ITO	y = 0.0451x + 0.13	—	—	Visual Estimate Approximate	p004 · Supporting Information · Fig. S5a

US-Ni-HITP-3 min/ITO electrode · Electrode

5.0 mM K3[Fe(CN)6] containing 0.1 M KCl; scan-rate dependent CV; effective catalytic activity surface area calculated from Ip-v^1/2 slope.

Temperature: 298
Geometry: three-electrode cell; Ni3(HITP)2 film/ITO working electrode, Ag/AgCl reference, Pt counter
Context: pristine Ni3(HITP)2 film on ITO electrode
Measurement source: p002 and p006 / 2376 and 2380 · Electrochemical measurements; Results and discussion · Fig. S5

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Effective catalytic activity surface area of US-Ni-HITP	0.236 cm2	—	—	Text Exact Reported	p006 / 2380 · Results and discussion · Fig. S5
Randles-Sevcik calibration slope for US-Ni-HITP-3 min/ITO	y = 0.0819x + 0.03	—	—	Visual Estimate Approximate	p004 · Supporting Information · Fig. S5b

DS-Ni-HITP-3 min/ITO electrode · Electrode

DS-Ni-HITP film in 2 mM glucose at scan rates from 20 to 200 mV s^-1.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Glucose oxidation process from scan-rate dependence	oxidation and reduction peak currents proportional to square root of scan rate	—	—	Qualitative Qualitative	p007 / 2381 · Results and discussion · Fig. 4f