Diffraction Structure — From non-conductive MOF to proton-conducting metal-HOFs: a new class of reversible transformations induced by solvent-free mechanochemistry

2 measurement groups · 8 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Mn-HOF-FA powder · Powder

PANalytical X'Pert PRO MPD, Cu source, Debye-Scherrer geometry, 4-90 deg 2theta, 20 h collection

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Mn-HOF-FA CCDC deposition number	2288811	—	—	SI Table Exact Reported	p007 · Table S1 · Table S1
Mn-HOF-FA unit cell volume	2518.81 A3	—	0.12 A3 in CIF	SI Table Exact Reported	Powder specimen and crystal data · CIF
Mn-HOF-FA final Rwp	0.0268	—	—	SI Table Exact Reported	p007 · Table S1 · Table S1
Mn-HOF-FA crystal system and space group	Monoclinic, An	—	—	SI Table Exact Reported	p007 · Table S1 · Table S1

Mn-HOF-MA powder · Powder

PANalytical X'Pert PRO MPD, Cu source, Debye-Scherrer geometry, 4-90 deg 2theta, 21 h 40 min collection

Temperature: 293
Atmosphere: Ambient
Geometry: 0.5 mm borosilicate capillary
Context: Target MHOF structure solution
Measurement source: p006-p007 · PXRD data collection and structure refinement details · Table S1

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Mn-HOF-MA CCDC deposition number	2288812	—	—	SI Table Exact Reported	p007 · Table S1 · Table S1
Mn-HOF-MA unit cell volume	1215.52 A3	—	—	SI Table Exact Reported	p007 · Table S1 · Table S1
Mn-HOF-MA final Rwp	0.0291	—	—	SI Table Exact Reported	p007 · Table S1 · Table S1
Mn-HOF-MA crystal system and space group	Monoclinic, P21/c	—	—	SI Table Exact Reported	p007 · Table S1 · Table S1