Microscopy Morphology — Stabilization of NASICON-Type Electrolyte against Li Anode via an Ionic Conductive MOF-Incorporated Adhesive Interlayer

Measurement evidence

Microscopy Morphology

Stabilization of NASICON-Type Electrolyte against Li Anode via an Ionic Conductive MOF-Incorporated Adhesive Interlayer · Zhao R., Gao L., Song M. et al. · ACS Energy Letters · 2021 · 3141-3150

4 measurement groups · 11 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

HIM/SEM-like morphology imaging

sintered LAGP pellet · Pellet

surface morphology of sintered LAGP pellet

Geometry
pellet surface
Context
pristine LAGP control
Measurement source
3143 · Results · Figure 1c
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
LAGP pellet diameter11 mmText
Exact Reported
1 · 1.1 Material synthesis
LAGP pellet thickness1.2 mmText
Exact Reported
1 · 1.1 Material synthesis
LAGP surface morphologyuneven surface formed by packed micro/nanosized crystalsText
Qualitative
3143 · Results · Figure 1c

Post-cycling cross-sectional and surface microscopy

ZCPL-LAGP electrolyte · Pellet

LAGP and ZCPL-LAGP after Li symmetric-cell cycling; tensile-force tearing test

Geometry
cycled Li/SSE interfaces
Context
composite and pristine control comparison
Measurement source
3146-3147 · Results · Figure 4d-i
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Unprotected LAGP post-cycling damagesevere cracks and surface spalling in LAGPText
Qualitative
3146 · Results · Figure 4d,e
ZCPL tensile morphologystretched and elongated into filamentous structure bridging LAGP and bulk ZCPLText
Qualitative
3146 · Results · Figures 4g and S20
ZIF-67 distribution in filamentous ZCPLhigh-density ZIF-67 within PEO matrixCaption
Qualitative
14 · Supplementary Figures · Figure S21
ZCPL-LAGP/Li post-cycling contactZCPL-LAGP and Li firmly combined owing to adhesivenessText
Qualitative
3146 · Results · Figure 4f

HIM/SEM cross-section and surface morphology

ZCPL-LAGP electrolyte · Pellet

ZCPL-coated LAGP surface and cross-section

Geometry
coated pellet
Context
composite MOF-polymer coated LAGP
Measurement source
3143-3144 · Results · Figure 1d,e
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
ZCPL coating thickness on LAGParound 25 umText
Approximate
3143 · Results · Figure 1e
ZCPL-LAGP surface morphologyrelatively flat and smooth surface after ZCPL coatingText
Qualitative
3143 · Results · Figure 1d

Helium ion microscopy (HIM)

as-obtained ZIF-67 nanoparticles · Powder

ZIF-67 morphology at different magnification

Geometry
nanoparticles
Context
pristine MOF component
Measurement source
2,4 · 1.2 Characterization; Supplementary Figures · Figure S2
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
ZIF-67 particle sizerelatively uniform size distribution around 400 nmCaption
Approximate
4 · Supplementary Figures · Figure S2
ZIF-67 morphologydodecahedron-shaped nanoparticlesCaption
Qualitative
4 · Supplementary Figures · Figure S2