Spectroscopy — Dual nanozyme based on ultrathin 2D conductive MOF nanosheets intergraded with gold nanoparticles for electrochemical biosensing of H2O2 in cancer cells

Measurement evidence

Spectroscopy

Dual nanozyme based on ultrathin 2D conductive MOF nanosheets intergraded with gold nanoparticles for electrochemical biosensing of H2O2 in cancer cells · Huang W., Xu Y., Wang Z. et al. · Talanta · 2022 · 123612

2 measurement groups · 8 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

FT-IR, Raman and UV-Vis spectroscopy

Au-NPs/Cu-HHTP-NSs · Nanosheet

Spectroscopic confirmation of Cu-O coordination and Au-NP surface plasmon response.

Context
pristine controls and Au-loaded composite
Measurement source
3-5 · 3.1. Characterization · Fig. 2b-d
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Au-NP interaction FT-IR shifted peaks3424 and 1621 cm-1Text
Exact Reported
3 · 3.1. Characterization · Fig. 2b
Cu-HHTP FT-IR characteristic peaks3450, 1635 and 1211 cm-1Text
Exact Reported
3 · 3.1. Characterization · Fig. 2b
Raman Cu-O coordination peak626 cm-1Text
Exact Reported
4 · 3.1. Characterization · Fig. 2c
Au-NP surface plasmon absorptionabout 520 nmText
Approximate
4 · 3.1. Characterization · Fig. 2d

X-ray photoelectron spectroscopy (XPS)

Au-NPs/Cu-HHTP-NSs · Nanosheet

Survey and high-resolution C 1s, Cu 2p and Au 4f spectra for Cu-HHTP-NSs and Au-NPs/Cu-HHTP-NSs.

Context
pristine nanosheet and composite
Measurement source
4-5 · 3.1. Characterization · Fig. 2g-i; Figure S9-S10
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Au XPS peaks in Au-NPs/Cu-HHTP-NSs84.0, 87.7, 333.6 and 352.4 eVText
Exact Reported
5 · 3.1. Characterization · Fig. 2i
Cu-HHTP-NSs Cu 2p peaks and gapCu 2p3/2 at 934 eV; Cu 2p1/2 at 953.8 eV; gap 19.8 eVText
Exact Reported
4 · 3.1. Characterization · Fig. 2h
Cu and O atomic contentsCu 5.75 at.% and O 23.53 at.%Text
Exact Reported
4 · 3.1. Characterization · Figure S9
XPS survey C/O/Cu peaks284.6, 531.7 and 934.5 eVText
Exact Reported
4 · 3.1. Characterization · Figure S9