Diffraction Structure — Conductive metal-organic framework synthesis from metal nanoparticle precursors

Measurement evidence

Diffraction Structure

Conductive metal-organic framework synthesis from metal nanoparticle precursors · Lister A.M., Wang Y., Armitage B.I. et al. · JPhys Materials · 2025 · 025004

3 measurement groups · 14 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Powder X-ray diffraction (PXRD)

Cu3(HITP)2 powder scraped from copper foil for PXRD · Powder

Rigaku Miniflex, Cu Kalpha 1.54 A; 2 to 50 deg at 5 deg min-1, 0.02 deg step.

Geometry
scraped powder from Cu foil scale-up
Context
pristine MOF powder with CuO side-product peaks
Measurement source
p005-p006 · Characterisation techniques; Results · Figure 3d
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
(001) peak position and sharpness(001) at 2theta = 27.5 deg; significantly sharper than typically reportedText
Exact Reported
p006 · Results and discussion · Figure 3d
CuO side-product PXRD peak2theta = 35.6 degText
Exact Reported
p006 · Results and discussion · Figure 3d
CuO side-product PXRD peak2theta = 38.6 degText
Exact Reported
p006 · Results and discussion · Figure 3d
hexagonal lattice parameter aa = b = 21.7 AText
Exact Reported
p006 · Results and discussion · Figure 3d
hexagonal lattice parameter ba = b = 21.7 AText
Exact Reported
p006 · Results and discussion · Figure 3d
hexagonal lattice parameter cc = 3.2 AText
Exact Reported
p006 · Results and discussion · Figure 3d
Cu3(HITP)2 PXRD MOF reflection at 2theta 12.62theta = 12.6 degText
Exact Reported
p006 · Results and discussion · Figure 3d
Cu3(HITP)2 PXRD MOF reflection at 2theta 16.62theta = 16.6 degText
Exact Reported
p006 · Results and discussion · Figure 3d
Cu3(HITP)2 PXRD MOF reflection at 2theta 27.42theta = 27.4 degText
Exact Reported
p006 · Results and discussion · Figure 3d
Cu3(HITP)2 PXRD MOF reflection at 2theta 4.72theta = 4.7 degText
Exact Reported
p006 · Results and discussion · Figure 3d
Cu3(HITP)2 PXRD MOF reflection at 2theta 9.62theta = 9.6 degText
Exact Reported
p006 · Results and discussion · Figure 3d
unassigned PXRD peakaround 24 degText
Approximate
p006 · Results and discussion · Figure 3d

Transmission electron microscopy

Cu3(HITP)2 powder from pure Cu metal for TEM · Powder

JEM-2100, 200 kV; MOF powder scraped from bulk metal and drop-cast onto Cu TEM grids with holey carbon film.

Geometry
TEM grid
Context
pristine MOF powder
Measurement source
p007 · Results and discussion · Figure 4a
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Cu3(HITP)2 interlayer spacingMarked as a best value within this paper3.2 AText
Exact Reported
p007 · Results and discussion · Figure 4a

Transmission electron microscopy

Ni3(HITP)2 powder from pure Ni metal for TEM · Powder

JEM-2100, 200 kV; MOF powder scraped from bulk metal and drop-cast onto Cu TEM grids with holey carbon film.

Geometry
TEM grid
Context
pristine MOF powder
Measurement source
p007 · Results and discussion · Figure 4b
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Ni3(HITP)2 interlayer spacingMarked as a best value within this paper3.3 AText
Exact Reported
p007 · Results and discussion · Figure 4b