Powder X-ray diffraction (PXRD)
Electrochemically synthesised Cu3(HHTP)2 scraped powder (from Cu tape scale-up) · Powder
Rigaku Miniflex, Cu Kalpha 1.54 A, 2-40 deg at 5 deg/min, 0.02 deg step; scraped powder from Cu-tape scale-up
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| PXRD hexagonal lattice parameter a=bMarked as a best value within this paper | a = b = 21.17 A | — | — | Text Exact Reported | 5 · 3.1 Preparation and Characterization · Figure 3d |
| PXRD hexagonal lattice parameter c (interlayer spacing)Marked as a best value within this paper | c = 3.21 A | — | — | Text Exact Reported | 5 · 3.1 Preparation and Characterization · Figure 3d |
| PXRD indexed peak position (001) | 2theta = 27.76 deg, assigned to (001) | — | — | Text Exact Reported | 5 · 3.1 Preparation and Characterization · Figure 3d |
| PXRD indexed peak position (100) | 2theta = 4.95 deg, assigned to (100) | — | — | Text Exact Reported | 5 · 3.1 Preparation and Characterization · Figure 3d |
| PXRD indexed peak position (200) | 2theta = 9.64 deg, assigned to (200) | — | — | Text Exact Reported | 5 · 3.1 Preparation and Characterization · Figure 3d |
| PXRD indexed peak position (210) | 2theta = 12.67 deg, assigned to (210) | — | — | Text Exact Reported | 5 · 3.1 Preparation and Characterization · Figure 3d |
| PXRD indexed peak position (220) | 2theta = 16.68 deg, assigned to (220) | — | — | Text Exact Reported | 5 · 3.1 Preparation and Characterization · Figure 3d |