Microscopy Morphology — Electrochemical Synthesis of Cu3(HHTP)2Metal–Organic Frameworks from Cu Nanoparticles for Chemiresistive Gas Sensing

Measurement evidence

Microscopy Morphology

Electrochemical Synthesis of Cu3(HHTP)2Metal–Organic Frameworks from Cu Nanoparticles for Chemiresistive Gas Sensing · Lister A.M., Armitage B.I., Wang Y. et al. · ACS Applied Nano Materials · 2025 · 15114-15121

1 measurement group · 3 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Scanning electron microscopy (SEM)

Electrochemically synthesised Cu3(HHTP)2 on Pt/glass IDE (2 h growth) · Electrode

Zeiss Merlin, InLens detector, 3 kV, 100 pA, 7 mm WD; separate samples at 0 min, 10 min, 2 h; ImageJ particle sizing

Atmosphere
vacuum (SEM)
Geometry
MOF-on-IDE at 0 min / 10 min / 2 h growth
Context
pristine framework growth (0 min panel is Cu-NP precursor)
Measurement source
5 · 3.2 Morphology and Resistance Studies · Figure 4
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Particle diameter, as-deposited Cu nanoparticles (0 min)15-20 nmrange 15-20 nmText
Range
5 · 3.2 Morphology and Resistance Studies · Figure 4b
Particle dimensions after 10 min growth40-65 nmrange 40-65 nmText
Range
5 · 3.2 Morphology and Resistance Studies · Figure 4d
Particle dimensions after 2 h growth60-160 nmrange 60-160 nmText
Range
5 · 3.2 Morphology and Resistance Studies · Figure 4f