Measurement evidence
Controlled synthesis of Cu-/Ni-based 1D c-MOFs and their application in near-linear temperature sensing · Zhang J., Xu C., Li J. et al. · Vacuum · 2023 · 111937
Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.
Cu1 · Powder
Field-emission SEM morphology assessment of as-synthesised powder.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| SEM morphology | 0.25 mL DMF, 3 h; relatively many nanoparticles and incomplete nanorods. | — | — | Text Qualitative | main p.4 · 3.1 Synthesis and characterization · Fig. 3 |
Cu10 · Powder
Field-emission SEM morphology assessment of as-synthesised powder.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| SEM morphology | 0.75 mL DMF, 6 h; more nanoparticles than 0.5 mL DMF samples. | — | — | Text Qualitative | main p.4 · 3.1 Synthesis and characterization · Fig. 3 |
Cu11 · Powder
Field-emission SEM morphology assessment of as-synthesised powder.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| SEM morphology | 0.75 mL DMF, 12 h; larger length-diameter-ratio nanostructures. | — | — | Text Qualitative | main p.4 · 3.1 Synthesis and characterization · Fig. 3 |
Cu12 · Powder
Field-emission SEM morphology assessment of as-synthesised powder.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| SEM morphology | 0.75 mL DMF, 24 h; wide structures with interconnected network structure. | — | — | Text Qualitative | main p.4 · 3.1 Synthesis and characterization · Fig. 3 |
Cu2 · Powder
Field-emission SEM morphology assessment of as-synthesised powder.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| SEM morphology | 0.25 mL DMF, 6 h; relatively many nanoparticles compared with 0.5 mL DMF samples. | — | — | Text Qualitative | main p.4 · 3.1 Synthesis and characterization · Fig. 3 |
Cu3 · Powder
Field-emission SEM morphology assessment of as-synthesised powder.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| SEM morphology | 0.25 mL DMF, 12 h; best morphology within 0.25 mL series according to discussion. | — | — | Text Qualitative | main p.4 · 3.1 Synthesis and characterization · Fig. 3 |
Cu4 · Powder
Field-emission SEM morphology assessment of as-synthesised powder.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| SEM morphology | 0.25 mL DMF, 24 h; nanorod morphology begins to degrade relative to 12 h. | — | — | Text Qualitative | main p.4 · 3.1 Synthesis and characterization · Fig. 3 |
Cu5 · Powder
Field-emission SEM morphology assessment of as-synthesised powder.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| SEM morphology | 0.50 mL DMF, 3 h; fewer nanoparticles than 0.25/0.75 mL at short time. | — | — | Text Qualitative | main p.4 · 3.1 Synthesis and characterization · Fig. 3 |
Cu6 · Powder
Field-emission SEM morphology assessment of as-synthesised powder.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| SEM morphology | 0.50 mL DMF, 6 h; nanorod-rich morphology. | — | — | Text Qualitative | main p.4 · 3.1 Synthesis and characterization · Fig. 3 |
Cu7 · Powder
Field-emission SEM morphology assessment of as-synthesised powder.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| SEM morphology | 0.50 mL DMF, 12 h; best Cu morphology and optimal sensor sample. | — | — | Text Qualitative | main p.4 · 3.1 Synthesis and characterization · Fig. 3 |
Cu8 · Powder
Field-emission SEM morphology assessment of as-synthesised powder.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| SEM morphology | 0.50 mL DMF, 24 h; nanorod degradation relative to 12 h. | — | — | Text Qualitative | main p.4 · 3.1 Synthesis and characterization · Fig. 3 |
Cu9 · Powder
Field-emission SEM morphology assessment of as-synthesised powder.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| SEM morphology | 0.75 mL DMF, 3 h; more nanoparticles than 0.5 mL DMF samples. | — | — | Text Qualitative | main p.4 · 3.1 Synthesis and characterization · Fig. 3 |
Ni1 · Powder
Field-emission SEM morphology assessment of as-synthesised powder.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| SEM morphology | Mixture of nanorods and nanoparticles due to short reaction time. | — | — | Text Qualitative | main p.3 · 3.1 Synthesis and characterization · Fig. 2 |
Ni2 · Powder
Field-emission SEM morphology assessment of as-synthesised powder.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| SEM morphology | Nanorods became the main morphology as nanoparticles decreased. | — | — | Text Qualitative | main p.3 · 3.1 Synthesis and characterization · Fig. 2 |
Ni3 · Powder
Field-emission SEM morphology assessment of as-synthesised powder.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| SEM morphology | Narrow and uniform nanorods. | — | — | Text Qualitative | main p.3 · 3.1 Synthesis and characterization · Fig. 2 |
Ni4 · Powder
Field-emission SEM morphology assessment of as-synthesised powder.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| SEM morphology | Scattered nanorods and granular structures after extended reaction. | — | — | Text Qualitative | main p.3 · 3.1 Synthesis and characterization · Fig. 2 |