Spectroscopy — Controlled synthesis of Cu-/Ni-based 1D c-MOFs and their application in near-linear temperature sensing

Measurement evidence

Spectroscopy

Controlled synthesis of Cu-/Ni-based 1D c-MOFs and their application in near-linear temperature sensing · Zhang J., Xu C., Li J. et al. · Vacuum · 2023 · 111937

2 measurement groups · 12 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

X-ray photoelectron spectroscopy (XPS, Escalab 250Xi)

Cu7 · Powder

Elemental and surface-state analysis of representative Cu3(HHTP)2.

Atmosphere
not reported
Context
pristine framework sensor/material
Measurement source
main p.5 · 3.1 Synthesis and characterization · Fig. 5e-h
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
C 1s C=C component284.8 eVText
Exact Reported
main p.5 · 3.1 Synthesis and characterization · Fig. 5
C 1s C-O component286.8 eVText
Exact Reported
main p.5 · 3.1 Synthesis and characterization · Fig. 5
Cu 2p Cu(I)-assigned binding energy932.8 eVText
Exact Reported
main p.5 · 3.1 Synthesis and characterization · Fig. 5
Cu 2p Cu(II)-assigned binding energy934.6 eVText
Exact Reported
main p.5 · 3.1 Synthesis and characterization · Fig. 5
O 1s C-O/C=O component532.9 eVText
Exact Reported
main p.5 · 3.1 Synthesis and characterization · Fig. 5
O 1s Cu-O-C/H component531.1 eVText
Exact Reported
main p.5 · 3.1 Synthesis and characterization · Fig. 5

X-ray photoelectron spectroscopy (XPS, Escalab 250Xi)

Ni3 · Powder

Elemental and surface-state analysis of representative Ni3(HHTP)2.

Atmosphere
not reported
Context
pristine framework sensor/material
Measurement source
main p.5 · 3.1 Synthesis and characterization · Fig. 5a-d
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
C 1s C-C component285 eVText
Exact Reported
main p.5 · 3.1 Synthesis and characterization · Fig. 5
C 1s C-O component287 eVText
Exact Reported
main p.5 · 3.1 Synthesis and characterization · Fig. 5
Ni 2p3/2 binding energy855.8 eVText
Exact Reported
main p.5 · 3.1 Synthesis and characterization · Fig. 5
O 1s C-O/C=O component532.9 eVText
Exact Reported
main p.5 · 3.1 Synthesis and characterization · Fig. 5
O 1s Ni-O-C/H component531.1 eVText
Exact Reported
main p.5 · 3.1 Synthesis and characterization · Fig. 5
Ni satellite binding energy860.7 eVText
Exact Reported
main p.5 · 3.1 Synthesis and characterization · Fig. 5