Partial recipeSource: Main
Route 1: Other
2019 · 2.7 Preparation and characterization of Ni3(HITP)2@PDA
Metal precursorsNi3(HITP)2 purchased powder
Linker precursorsHITP already present in purchased Ni3(HITP)2; dopamine hydrochloride/PDA solution for coating
Solventsethanol; double-distilled water
Additives25% ammonia solution; PDA solution
Atmospherenot specified
Temperatureroom temperature
Time0.1667 h ultrasonication + 0.1667 h stirring + 0.333 h after ammonia + 3 h after PDA addition
Oxidant / reductantammonia-assisted dopamine/PDA coating; oxidant/reductant not specified
Work-upwashed by centrifugation with double-distilled water and ethanol at 10000 rps for 10 min, repeated three times
Activationdried for further use; drying temperature/atmosphere not specified
Show 5 structured reagent records
| Role | Reagent | Amount / concentration | Source |
|---|---|---|---|
| Other | Ni3(HITP)2 | 5 mg | 2019 · 2.7 Preparation and characterization of Ni3(HITP)2@PDA |
| Solvent | ethanol | 5 mL initially; 3 mL added later | 2019 · 2.7 Preparation and characterization of Ni3(HITP)2@PDA |
| Solvent | double-distilled water | 18 mL | 2019 · 2.7 Preparation and characterization of Ni3(HITP)2@PDA |
| Base | ammonia solution | 600 mL as OCR text; likely 600 uL but not corrected in extracted record · 25% | 2019 · 2.7 Preparation and characterization of Ni3(HITP)2@PDA |
| Additive | PDA solution | 2 mL · 50 mg mL^-1 | 2019 · 2.7 Preparation and characterization of Ni3(HITP)2@PDA |