X-ray photoelectron spectroscopy (XPS)
Free-standing Ni3(HITP)2 membrane · Thin Film
Thermo Scientific ESCALAB 250 Xi XPS; baseline correction by Avantage; apparent charging normalised to C 1s = 284.8 eV.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| Ni-species impurity assessment | Ni metal, NiO and Ni(OH)2 impurities ruled out in the thin layer close to SiO2 | — | — | Text Qualitative | main p.2 / article p.1361 · Results and discussion · Figures S6,S7 |
| Ni 2p3/2 binding energy in Ni3(HITP)2 top surface | 855.5 eV | — | — | Text Exact Reported | main p.2 / article p.1361 · Results and discussion · Figure S7 |