Microscopy Morphology — Tunable Carrier Type of a Semiconducting 2D Metal-Organic Framework Cu3(HHTP)2

4 measurement groups · 9 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

As-electrodeposited Cu3(HHTP)2 thin film on Au/SiO2 · Thin Film

Elemental analysis of electrodeposited Cu3(HHTP)2 film.

Context: Pristine electrodeposited film.
Measurement source: main p.3, article p.12406 · Results and Discussion · Figure S2

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
EDS detected elements in electrodeposited film	Cu, O and C detected; atomic ratio in good agreement with Cu3C36H18O12	—	—	Text Qualitative	main p.3, article p.12406 · Results and Discussion · Figure S2

As-electrodeposited Cu3(HHTP)2 thin film on Au/SiO2 · Thin Film

Top-view and cross-sectional SEM of as-electrodeposited Cu3(HHTP)2.

Context: Pristine electrodeposited film.
Measurement source: main p.3, article p.12406 · Results and Discussion · Figure 3; Figure S1

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Electrodeposited film thickness	ca. 5 um	—	—	Text Approximate	main p.3, article p.12406 · Results and Discussion · Figure S1
Aggregated nanorod average width	86 nm	—	—	Text Rounded Reported	main p.3, article p.12406 · Results and Discussion · Figure 3b
As-electrodeposited spherical particle diameter	ca. 6 um	—	—	Text Approximate	main p.3, article p.12406 · Results and Discussion · Figure 3a

CuHHTP-PAA-40 PAA-transferred Cu3(HHTP)2 film · Thin Film

PAA-transferred Cu3(HHTP)2 film visual and cross-sectional characterisation.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
PAA-transferred film EDS carbon atomic percentage	71.76%	—	—	Visual Estimate Approximate	SI p.S7 · Figure S5 · Figure S5b
PAA-transferred film EDS copper atomic percentage	4.93%	—	—	Visual Estimate Approximate	SI p.S7 · Figure S5 · Figure S5b
PAA-transferred film EDS oxygen atomic percentage	23.32%	—	—	Visual Estimate Approximate	SI p.S7 · Figure S5 · Figure S5b

CuHHTP-70 PMMA-transferred Cu3(HHTP)2 film · Thin Film

SEM images of PMMA-transferred Cu3(HHTP)2 films dried at 40 C and 70 C.

Context: PMMA-supported composite films.
Measurement source: main p.4, article p.12407 · Results and Discussion · Figure 3c,d

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
CuHHTP-40 surface morphology	Flattened compact surface with clear interparticle connectivity	—	—	Text Qualitative	main p.3, article p.12406 · Results and Discussion · Figure 3c
CuHHTP-70 surface morphology	Rougher and more disrupted surface; brighter zones attributed to PMMA charging/residues	—	—	Text Qualitative	main p.5, article p.12408 · Charge Transport Properties · Figure 3d