Microscopy Morphology — Large-Area Synthesis of Ultrathin, Flexible, and Transparent Conductive Metal–Organic Framework Thin Films via a Microfluidic-Based Solution Shearing Process

Measurement evidence

Microscopy Morphology

Large-Area Synthesis of Ultrathin, Flexible, and Transparent Conductive Metal–Organic Framework Thin Films via a Microfluidic-Based Solution Shearing Process · Lee T., Kim J.-O., Park C. et al. · Advanced Materials · 2022 · 2107696

3 measurement groups · 6 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

SEM, cross-sectional SEM, HRTEM, STEM-EDS

MASS-PRC Ni3(HITP)2 thin film · Thin Film

Morphology and elemental mapping of MASS-PRC Ni3(HITP)2 thin film.

Context
pristine Ni3(HITP)2 thin film
Measurement source
2 · 2.1 Preparation of Ni3(HITP)2 Thin Film · Figure 1f,i-k
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Average Ni3(HITP)2 crystallite sizeabout 30 nmText
Approximate
2 · 2.1 Preparation of Ni3(HITP)2 Thin Film · Figure 1f

HAADF-STEM

Ni3(HITP)2@Pt thin film · Thin Film

Imaging of Ni3(HITP)2 film with atomically dispersed Pt atoms.

Context
Pt-doped/composite Ni3(HITP)2 thin film
Measurement source
35 · Figure S21 · Figure S21
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Atomically dispersed Pt observedHAADF-STEM image shows Ni3(HITP)2 with atomically dispersed Pt atomsCaption
Qualitative
35 · Figure S21 caption · Figure S21

AFM topography and scratched-film thickness/roughness analysis

MASS-PRC Ni3(HITP)2 thin film · Thin Film

Film thickness and roughness measured for shearing speeds 0.02-0.10 mm/s.

Context
pristine Ni3(HITP)2 thin film
Measurement source
5 · 2.2 Characterizations of Ni3(HITP)2 Thin Film · Figure 3c; Figures S18-S19
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Ra at 0.02 mm/s shearing speed4.779 nmCaption
Exact Reported
33 · Figure S19 caption · Figure S19
Ra roughness range across shearing speeds3.792-4.779 nmCaption
Range
33 · Figure S19 caption · Figure S19
Thickness range controlled by shearing speed11 to 64 nmText
Range
5 · 2.2 Characterizations of Ni3(HITP)2 Thin Film · Figure 3c
Thickness-shearing speed power-law exponentpower of -1.09Text
Exact Reported
5 · 2.2 Characterizations of Ni3(HITP)2 Thin Film · Figure 3c