Measurement evidence
A Novel Electrically Conductive Perylene Diimide-Based MOF-74 Series Featuring Luminescence and Redox Activity · Scheurle P.I., Biewald A., Mahringer A. et al. · Small Structures · 2022 · 2100195
Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.
PDI-MOF-74(Zn) VAC film on glass · Thin Film
PDI-MOF-74(Zn) film grown on glass by VAC; diffraction confirms crystalline film with random crystallite distribution
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| film crystallinity | crystalline film with random crystallite distribution | — | — | Text Qualitative | 3 · Results and Discussion · Figures S28-S29 |
PDI-MOF-74(Mg) powder · Powder
Bruker D8, Cu Kalpha; simulated MOF-74 model refined to experimental PXRD; best refinements in triclinic P1
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| triclinic lattice parameter a | 72.6294 A | — | — | Text Exact Reported | 10, 20-21 · Unit cell parameters |
| triclinic lattice parameter b | 74.5613 A | — | — | Text Exact Reported | 10, 20-21 · Unit cell parameters |
| triclinic lattice parameter c | 5.5891 A | — | — | Text Exact Reported | 10, 20-21 · Unit cell parameters |
| pi-pi stacking distance between adjacent PDI cores | 3.4 A | — | — | Text Rounded Reported | 3 · Results and Discussion · Figure 2 |
| modelled hexagonal channel aperture | 4.0-4.5 nm | — | — | Text Range | 3 · Results and Discussion · Figure 1; Figure S1 |
| pronounced PXRD reflections | 2.45, 3.97, 4.76, 6.31, 8.18, 10.66, 11.97 degrees 2theta | — | — | Text Exact Reported | 2 · Results and Discussion · Figure 2 |
| Pawley Rp triclinic refinement | 2.29% | — | — | Text Exact Reported | 10, 20-21 · Unit cell parameters |
| Pawley Rwp triclinic refinement | 3.23% | — | — | Text Exact Reported | 10, 20-21 · Unit cell parameters |
PDI-MOF-74(Ni) powder · Powder
Bruker D8, Cu Kalpha; simulated MOF-74 model refined to experimental PXRD; best refinements in triclinic P1
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| triclinic lattice parameter a | 72.2829 A | — | — | Text Exact Reported | 10, 20-21 · Unit cell parameters |
| triclinic lattice parameter b | 75.6727 A | — | — | Text Exact Reported | 10, 20-21 · Unit cell parameters |
| triclinic lattice parameter c | 5.5574 A | — | — | Text Exact Reported | 10, 20-21 · Unit cell parameters |
| pi-pi stacking distance between adjacent PDI cores | 3.3 A | — | — | Text Rounded Reported | 3 · Results and Discussion · Figure 2 |
| modelled hexagonal channel aperture | 4.0-4.5 nm | — | — | Text Range | 3 · Results and Discussion · Figure 1; Figure S1 |
| pronounced PXRD reflections | 2.45, 3.97, 6.31, 8.04/8.48, 10.35/10.88, 11.70 degrees 2theta | — | — | Text Exact Reported | 2 · Results and Discussion · Figure 2 |
| Pawley Rp triclinic refinement | 2.75% | — | — | Text Exact Reported | 10, 20-21 · Unit cell parameters |
| Pawley Rwp triclinic refinement | 3.96% | — | — | Text Exact Reported | 10, 20-21 · Unit cell parameters |
PDI-MOF-74(Zn) powder · Powder
Bruker D8, Cu Kalpha; simulated MOF-74 model refined to experimental PXRD; best refinements in triclinic P1
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| triclinic lattice parameter a | 72.6294 A | — | — | Text Exact Reported | 10, 20-21 · Unit cell parameters |
| triclinic lattice parameter b | 74.5613 A | — | — | Text Exact Reported | 10, 20-21 · Unit cell parameters |
| triclinic lattice parameter c | 5.5891 A | — | — | Text Exact Reported | 10, 20-21 · Unit cell parameters |
| pi-pi stacking distance between adjacent PDI cores | 3.4 A | — | — | Text Rounded Reported | 3 · Results and Discussion · Figure 2 |
| modelled hexagonal channel aperture | 4.0-4.5 nm | — | — | Text Range | 3 · Results and Discussion · Figure 1; Figure S1 |
| pronounced PXRD reflections | 2.45, 3.97, 8.10, 10.52, 12.01 degrees 2theta | — | — | Text Exact Reported | 2 · Results and Discussion · Figure 2 |
| Pawley Rp triclinic refinement | 1.56% | — | — | Text Exact Reported | 10, 20-21 · Unit cell parameters |
| Pawley Rwp triclinic refinement | 2.38% | — | — | Text Exact Reported | 10, 20-21 · Unit cell parameters |