Microscopy Morphology — High performance metal–organic-framework coatings obtained via thermal gradient synthesis

Measurement evidence

Microscopy Morphology

High performance metal–organic-framework coatings obtained via thermal gradient synthesis · Jeremias F., Henninger S.K., Janiak C. · Chemical Communications · 2012 · 9708-9710

1 measurement group · 3 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Optical microscopy and SEM/EDX

Scanning electron microscopy Elemental microanalysis and mapping

HKUST-1 coating on 5 cm x 5 cm copper sheet · Thin Film

SEM/EDX on FEI Quanta 400 MkII; top-down images under high vacuum; cross sections in environmental mode, H2O 100 Pa.

Atmosphere: high vacuum for top-down SEM; environmental H2O 100 Pa for cross-section images
Geometry: top-down coating and polished cross-section embedded in polymer resin
Context: whole MOF coating on Cu
Measurement source: 3 · SEM/EDX Conditions · Figures S2-S3

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
crystallite size upper boundMarked as a best value within this paper	less than 10 um	—	upper bound	Text Approximate	9709 · Results · Figure 2
macropore-like channel diameter lower bound	30 to 50 um	—	range lower bound	Text Range	9710 · Results · Figure 2c; Figure S8
macropore-like channel diameter upper bound	30 to 50 um	—	range upper bound	Text Range	9710 · Results · Figure 2c; Figure S8