Microscopy Morphology — Charge. transport, conductivity and Seebeck coefficient in pristine and TCNQ loaded preferentially grown metal-organic framework films

Measurement evidence

Microscopy Morphology

Charge. transport, conductivity and Seebeck coefficient in pristine and TCNQ loaded preferentially grown metal-organic framework films · Chen X., Zhang K., Hassan Z.M. et al. · Journal of Physics Condensed Matter · 2022 · 404001

3 measurement groups · 6 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Planar FE-SEM

Random polycrystalline pristine HKUST-1 SURMOF film on borosilicate glass, ca. 130 nm · Thin Film

Planar morphology of pristine and TCNQ-loaded HKUST-1 films on borosilicate glass after 10 and 40 cycles.

Geometry
top-down thin-film morphology
Context
pristine and guest-loaded random polycrystalline films
Measurement source
article pages 5 and 8 · Figure 4 and 1.2 Thin-film electrical conductometry · Figure 4
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Borosilicate film thickness after 10 cyclesapproximately 40 nm40 nmText
Approximate
article page 8 · 1.2 Thin-film electrical conductometry · Figure 4
Borosilicate film thickness after 40 cyclesapproximately 130 nm130 nmText
Approximate
article page 8 · 1.2 Thin-film electrical conductometry · Figures 4 and 10

FE-SEM cross-sectional imaging, Hitachi S 4700 operated at 5 kV

Preferentially (001)-oriented pristine HKUST-1 SURMOF film, 100 nm · Thin Film

Cross sections of HKUST-1 SURMOF films on silicon substrates for thickness calibration across spray cycles.

Geometry
thin film cross-section on Al-SEM cross-section holder
Context
pristine framework thickness series
Measurement source
article page 4 · Figure 3 and surrounding text · Figure 3
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Film thickness after 15 LPE spray cyclesapproximately 40 nm40 nmText
Approximate
article page 4 · Figure 3 discussion · Figure 3
Film thickness after 25 LPE spray cyclesapproximately 60 nm60 nmText
Approximate
article page 4 · Figure 3 discussion · Figure 3
Film thickness after 30 LPE spray cyclesapproximately 70 nm70 nmText
Approximate
article page 4 · Figure 3 discussion · Figure 3
Film thickness after 45 LPE spray cyclesapproximately 100 nm100 nmText
Approximate
article page 4 · Figure 3 discussion · Figure 3

Top-down planar FE-SEM

Random polycrystalline pristine HKUST-1 SURMOF film on hydroxyl-terminated SiO2/Si · Thin Film

Pristine and TCNQ-loaded random polycrystalline HKUST-1 films on hydroxyl-terminated SiO2/Si.

Geometry
top-down thin-film morphology
Context
pristine and guest-loaded compact films
Measurement source
article page 8 · 1.2 Thin-film electrical conductometry · Figure 5
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource