Spectroscopy — Adjustable Synthesis of Ni-Based Metal-Organic Framework Membranes and Their Field-Effect Transistor Sensors for Mercury Detection

Measurement evidence

Spectroscopy

Adjustable Synthesis of Ni-Based Metal-Organic Framework Membranes and Their Field-Effect Transistor Sensors for Mercury Detection · Shen S., Tan P., Tang Y. et al. · ACS Applied Electronic Materials · 2022 · 622-630

2 measurement groups · 6 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

TGA

Thermogravimetric analysis

S4 Ni3(HITP)2 membrane · Thin Film

Thermogravimetric analysis at 10 deg C/min in air.

Atmosphere: air
Context: pristine Ni3(HITP)2 sample
Measurement source: 626 · 2.5 Characterization; 3.1 · Figure S5

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
TGA weight-loss/decomposition onset	about 200 deg C	—	about	Text Approximate	626 · 3.1. Structural and Morphological Characteristics · Figure S5
TGA labelled weight loss	71% weight loss labelled in Figure S5	—	—	Figure Axis Approximate	S-7 · Figure S5 · Figure S5

XPS

X-ray photoelectron spectroscopy

S4 Ni3(HITP)2 membrane · Thin Film

XPS survey and high-resolution Ni 2p, N 1s and O 1s spectra of S4 sample.

Context: pristine Ni3(HITP)2 membrane
Measurement source: S-6 · Figure S4 caption · Figure S4

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
C 1s XPS peak	284.8 eV	—	—	Text Rounded Reported	626 · 3.1. Structural and Morphological Characteristics · Figure S4
N 1s XPS peak	399.3 eV	—	—	Text Rounded Reported	626 · 3.1. Structural and Morphological Characteristics · Figure S4
Ni 2p XPS peak	855.6 eV	—	—	Text Rounded Reported	626 · 3.1. Structural and Morphological Characteristics · Figure S4
O 1s XPS peak	532.3 eV	—	—	Text Rounded Reported	626 · 3.1. Structural and Morphological Characteristics · Figure S4