Microscopy Morphology — Self-assembly and optoelectronic properties of isoreticular MOF nanocrystals

4 measurement groups · 7 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

IRMOF-8 microstructures cast from butanone · Thin Film

Morphology after dispersing original microstructures in butanone, drop casting and annealing at 100 C for 5 min.

Context: pristine framework solvent-processed morphology sample
Measurement source: 110 · 3.2. Solvents dependent self-assembly and their morphology studies · Fig. 4(c,d)

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
butanone-cast morphology	smooth platelets; no distinct nanocrystal arrangement or void spaces by TEM	—	—	Text Qualitative	110 · 3.2. Solvents dependent self-assembly and their morphology studies · Fig. 4(c,d)

as-prepared IRMOF-8 microstructures in DMF · Powder

Morphology of microstructures as prepared in DMF.

Context: pristine framework morphology sample
Measurement source: 110 · 3.2. Solvents dependent self-assembly and their morphology studies · Fig. 4(a,b)

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
as-prepared DMF microstructure average length upper bound	~2-4 um	4 um	~	Text Range	110 · 3.2. Solvents dependent self-assembly and their morphology studies · Fig. 4(a)
as-prepared DMF microstructure average length lower bound	~2-4 um	2 um	~	Text Range	110 · 3.2. Solvents dependent self-assembly and their morphology studies · Fig. 4(a)
as-prepared DMF microstructure average width upper bound	~1-2 um	2 um	~	Text Range	110 · 3.2. Solvents dependent self-assembly and their morphology studies · Fig. 4(a)
as-prepared DMF microstructure average width lower bound	~1-2 um	1 um	~	Text Range	110 · 3.2. Solvents dependent self-assembly and their morphology studies · Fig. 4(a)

IRMOF-8 microstructures cast from DMF/propanol · Thin Film

Morphology after dispersing original microstructures in DMF/propanol, drop casting and annealing at 100 C for 5 min.

Context: pristine framework solvent-processed morphology sample
Measurement source: 110 · 3.2. Solvents dependent self-assembly and their morphology studies · Fig. 4(g,h)

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
DMF/propanol-cast morphology	thick cubes with smooth surfaces; TEM shows self-assembled cubic nanocrystals inside larger thick cubes	—	—	Text Qualitative	110 · 3.2. Solvents dependent self-assembly and their morphology studies · Fig. 4(g,h)

IRMOF-8 microstructures cast from toluene · Thin Film

Morphology after dispersing original microstructures in toluene, drop casting and annealing at 100 C for 5 min.

Context: pristine framework solvent-processed morphology sample
Measurement source: 110 · 3.2. Solvents dependent self-assembly and their morphology studies · Fig. 4(e,f)

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
toluene-cast morphology	smooth platelets; no distinct nanocrystal arrangement or void spaces by TEM	—	—	Text Qualitative	110 · 3.2. Solvents dependent self-assembly and their morphology studies · Fig. 4(e,f)