Diffraction Structure — Conductive Metal-Organic Framework Thin Film Hybrids by Electropolymerization of Monosubstituted Acetylenes

Measurement evidence

Diffraction Structure

Conductive Metal-Organic Framework Thin Film Hybrids by Electropolymerization of Monosubstituted Acetylenes · Klyatskaya S., Kanj A.B., Molina-Jiron C. et al. · ACS Applied Materials and Interfaces · 2020 · 30972-30979

1 measurement group · 5 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Out-of-plane X-ray diffraction

X-ray diffraction and scattering

BPA@Cu(BDC)-SURMOF-2 after electropolymerisation · Electrode

D8-Advance Bruker AXS diffractometer, Cu K-alpha radiation, theta-theta geometry, position sensitive detector, variable divergence slit.

Geometry: SURMOF thin film before loading, after 1-hexyne exposure, and after EP; also film on interdigitated electrode
Context: pristine, guest-loaded, blank EP, and electropolymerised samples compared
Measurement source: SI p.S-3 · X-ray Diffraction (XRD) · Figure 2b; Figure S2

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Approximate Cu(BDC) SURMOF (100) XRD peak	about 8.3 degrees 2 theta	—	visual estimate from plot axis	Figure Axis Approximate	main p.3 · Results and Discussion · Figure 2b
Approximate Cu(BDC) SURMOF (200) XRD peak	about 16.7 degrees 2 theta	—	visual estimate from plot axis	Figure Axis Approximate	main p.3 · Results and Discussion · Figure 2b
Approximate Cu(BDC) SURMOF (300) XRD peak	about 24.8 degrees 2 theta	—	visual estimate from plot axis	Figure Axis Approximate	main p.3 · Results and Discussion · Figure 2b
XRD peak positions after EP	No further changes in diffraction peak positions; intensities slightly reduced	—	—	Text Qualitative	main p.4 · Results and Discussion · Figure 2b
XRD after 1-hexyne immersion	No major differences to pristine film	—	—	Text Qualitative	main p.3 · Results and Discussion · Figure S2