Other — Electrochemical synthesis of metal organic framework films with proton conductive property

Measurement evidence

Other

Electrochemical synthesis of metal organic framework films with proton conductive property · Zhang F., Zhang T., Zou X. et al. · Solid State Ionics · 2017 · 125-132

3 measurement groups · 15 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

ICP-AES of Cu2+ in solution

as-prepared NENU-3 films on copper · Thin Film

Copper slice as anodic electrode at 2.0 V for 0.5-8 h.

Geometry
electrochemical synthesis solution
Context
synthesis solution for target framework
Measurement source
4-5 · Table 2; Synthesis and characterizations · Table 2
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Cu2+ concentration at 2.0 V for 0.5 h59.7 mg L-1Table
Exact Reported
4 · Table 2 · Table 2
Cu2+ concentration at 2.0 V for 1 h117.0 mg L-1Table
Exact Reported
4 · Table 2 · Table 2
Cu2+ concentration at 2.0 V for 2 h467.0 mg L-1Table
Exact Reported
4 · Table 2 · Table 2
Cu2+ concentration at 2.0 V for 4 h1030.0 mg L-1Table
Exact Reported
4 · Table 2 · Table 2
Cu2+ concentration at 2.0 V for 6 h1195.0 mg L-1Table
Exact Reported
4 · Table 2 · Table 2
Cu2+ concentration at 2.0 V for 8 h1260.0 mg L-1Table
Exact Reported
4 · Table 2 · Table 2

ICP-AES of Cu2+ in solution

as-prepared NENU-3 films on copper · Thin Film

Copper slice as anodic electrode at different applied voltages for 2 h.

Geometry
electrochemical synthesis solution
Context
synthesis solution for target framework
Measurement source
3,5 · Table 1; Synthesis and characterizations · Table 1
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Cu2+ concentration at 1.0 V for 2 h16.7 mg L-1Table
Exact Reported
3 · Table 1 · Table 1
Cu2+ concentration at 2.0 V for 2 h467.0 mg L-1Table
Exact Reported
3 · Table 1 · Table 1
Cu2+ concentration at 5.0 V for 2 h1220.0 mg L-1Table
Exact Reported
3 · Table 1 · Table 1
Cu2+ concentration at 8.0 V for 2 h1545.0 mg L-1Table
Exact Reported
3 · Table 1 · Table 1

Thermogravimetric analysis (TGA), Mettler Toledo TGA 2, 25-700 deg C, 1 deg C min-1, dry air

as-prepared NENU-3 films on copper · Thin Film

Thermal stability of NENU-3 material.

Temperature
298-973
Atmosphere
dry air
Geometry
powder/film material
Context
guest-loaded target framework
Measurement source
2,6 · Characterizations; Stability · Fig. 6A
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
decomposition completeabout 500 deg CText
Approximate
6 · Stability · Fig. 6A
decomposition onsetaround 285 deg CText
Approximate
6 · Stability · Fig. 6A
first water-loss eventaround 80 deg CText
Approximate
6 · Stability · Fig. 6A
second water-loss eventaround 120 deg CText
Approximate
6 · Stability · Fig. 6A
thermal stability limitup to 280 deg CText
Rounded Reported
6 · Stability · Fig. 6A