Spectroscopy — Electrochemical synthesis of metal organic framework films with proton conductive property

Measurement evidence

Spectroscopy

Electrochemical synthesis of metal organic framework films with proton conductive property · Zhang F., Zhang T., Zou X. et al. · Solid State Ionics · 2017 · 125-132

2 measurement groups · 9 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

FT-IR, Bruker IF66F/V, KBr pellets, 400-4000 cm-1

NENU-3 film, 2.0 V for 8 h · Thin Film

FT-IR of NENU-3 powders collected from corresponding films prepared at 8.0 h and 2.0 V.

Temperature
room temperature
Geometry
powder from film
Context
guest-loaded target framework
Measurement source
SI · Supporting Information · Figure S1
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
FT-IR characteristic band nu(P-O)1080 cm-1Text
Exact Reported
6 · Synthesis and characterizations · Fig. S1
FT-IR characteristic band nu(W-O-W)827 cm-1Text
Exact Reported
6 · Synthesis and characterizations · Fig. S1
FT-IR characteristic band nu(W-O-W)898 cm-1Text
Exact Reported
6 · Synthesis and characterizations · Fig. S1
FT-IR characteristic band nu(W-O)982 cm-1Text
Exact Reported
6 · Synthesis and characterizations · Fig. S1

XPS W 4f and 5p3/2 spectra, Scienta ESCA200

NENU-3 film, 2.0 V for 8 h · Thin Film

Comparison of pure PTA and NENU-3 material collected from film prepared at 2.0 V for 8 h.

Geometry
powder collected from film
Context
guest-loaded target framework with pure PTA reference
Measurement source
5-6 · Synthesis and characterizations · Fig. 5
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
NENU-3 W 4f5/2 binding energy38.0 eVText
Exact Reported
5-6 · Synthesis and characterizations · Fig. 5
NENU-3 W 4f7/2 binding energy36.0 eVText
Exact Reported
5-6 · Synthesis and characterizations · Fig. 5
PTA W 4f5/2 binding energy38.0 eVText
Exact Reported
5-6 · Synthesis and characterizations · Fig. 5
PTA W 4f7/2 binding energy36.2 eVText
Exact Reported
5-6 · Synthesis and characterizations · Fig. 5
PTA W 5p3/2 binding energy39.8 eVText
Exact Reported
5-6 · Synthesis and characterizations · Fig. 5