Spectroscopy — Novel 2D CuFe-MOF-based immunoprobe: Addressing antifouling electrochemical immunosensing inadequate sensitivity challenge

Measurement evidence

Spectroscopy

Novel 2D CuFe-MOF-based immunoprobe: Addressing antifouling electrochemical immunosensing inadequate sensitivity challenge · Jiang X., Yao T., Wang S. et al. · Sensors and Actuators B: Chemical · 2024 · 135410

4 measurement groups · 9 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

FTIR

Au-Thi@ST-HA hydrogel · Thin Film

FTIR spectra of ST, HA and ST-HA gel to verify amide-bond formation.

Context
hydrogel substrate
Measurement source
3 · 3.2 Verification of the construction of antifouling hydrogel · Fig. 1B
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
ST-HA gel N-H bending peak1550 cm-1Text
Rounded Reported
3 · 3.2 Verification of hydrogel · Fig. 1B
HA carboxyl C=O peak1650 cm-1Text
Rounded Reported
3 · 3.2 Verification of hydrogel · Fig. 1B

UV-visible spectroscopy

CuFe-MOF feed-ratio series · Nanosheet

Compared peroxidase-like activity of CuFe-MOF materials with different Cu:Fe feed ratios from Cu-BDC to 1:2.

Context
target mixed-metal MOF ratio optimisation
Measurement source
5 · 3.3 Characterization of immunoprobe · Fig. 2L
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Peroxidase-like activity wavelength range550-750 nmText
Range
5 · 3.3 Characterization of immunoprobe · Fig. 2L
Optimal Cu:Fe feed ratioMarked as a best value within this paperCu:Fe = 1:0.5Text
Exact Reported
5 · 3.3 Characterization of immunoprobe · Fig. 2L

X-ray photoelectron spectroscopy (XPS)

Cu-BDC nanosheets · Nanosheet

Fe 2p and Cu 2p spectra for Cu-BDC.

Context
pristine Cu-BDC control
Measurement source
5 · 3.3 Characterization of immunoprobe · Fig. 2D,E
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Cu-BDC Cu 2p binding energy934.7 eVFigure Axis
Rounded Reported
5 · 3.3 Characterization of immunoprobe · Fig. 2E

X-ray photoelectron spectroscopy (XPS)

2D CuFe-MOF · Nanosheet

Fe 2p and Cu 2p spectra for CuFe-MOF.

Context
target mixed-metal MOF
Measurement source
4 · 3.3 Characterization of immunoprobe · Fig. 2F,G
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Fe introduction into nanosheetsFe successfully introduced into nanosheetsText
Qualitative
4 · 3.3 Characterization of immunoprobe · Fig. 2D-G; Fig. S2
CuFe-MOF Cu 2p binding energy934.5 eVFigure Axis
Rounded Reported
5 · 3.3 Characterization of immunoprobe · Fig. 2G
CuFe-MOF Fe 2p1/2 binding energy724.1 eVFigure Axis
Rounded Reported
5 · 3.3 Characterization of immunoprobe · Fig. 2F
CuFe-MOF Fe 2p3/2 binding energy714.6 eVFigure Axis
Rounded Reported
5 · 3.3 Characterization of immunoprobe · Fig. 2F