Measurement evidence
Ammonia-Assisted Chemical Vapor Deposition Growth of Two-Dimensional Conjugated Coordination Polymer Thin Films · Liu J., Fu S., Fu Y. et al. · Journal of the American Chemical Society · 2025 · 18190-18196
Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.
Cu-BHT-w NH3-assisted CVD thin film · Thin Film
Cu-BHT-w structural/morphological confirmation and PXRD comparison with Cu-BHT-o.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| S-H Raman peak absence | S-H peak at ~2500 cm^-1 absent | — | — | Caption Qualitative | SI p31 · Figure S25 caption · Figure S25c |
Cu-HHB-w NH3-assisted CVD thin film · Thin Film
Cu-HHB-w structural/morphological confirmation and PXRD comparison with Cu-HHB-o.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| O-H Raman peak absence | O-H peak at ~3300 cm^-1 absent | — | — | Caption Qualitative | SI p29 · Figure S23 caption · Figure S23c |
Fe-HHB-o CVD thin film without NH3 · Thin Film
GIWAXS at SOLEIL SIRIUS; beam energy 10 keV; incidence angle 0.12 deg; six 30 s images.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| crystal domain area | ~10^2 nm2 | — | — | Text Approximate | 18192 · Results and Discussion · Figure 3b; Figure S9 |
| GIWAXS FWHM for (001) peak | 0.044 Angstrom^-1 | — | — | Caption Exact Reported | SI p17 · Figure S11 caption · Figure S11b |
| GIWAXS FWHM for (100) peak | 0.033 Angstrom^-1 | — | — | Caption Exact Reported | SI p17 · Figure S11 caption · Figure S11a |
| GIWAXS FWHM for (200) peak | 0.035 Angstrom^-1 | — | — | Caption Exact Reported | SI p17 · Figure S11 caption · Figure S11c |
| GIWAXS FWHM for (210) peak | 0.036 Angstrom^-1 | — | — | Caption Exact Reported | SI p17 · Figure S11 caption · Figure S11d |
Fe-HHB-w NH3-assisted CVD thin film · Thin Film
GIWAXS at ESRF ID10; beam energy 22 keV; incidence angle 0.09 deg; 10 s exposure.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| GIWAXS Qz (001) peak | Qz = 1.53 Angstrom^-1 | — | — | Text Exact Reported | 18192 · Results and Discussion · Figure 3c |
| GIWAXS Qxy (100) peak | Qxy = 0.96 Angstrom^-1 | — | — | Text Exact Reported | 18192 · Results and Discussion · Figure 3c |
| GIWAXS Qxy (200) peak | Qxy = 1.92 Angstrom^-1 | — | — | Text Exact Reported | 18192 · Results and Discussion · Figure 3c |
| GIWAXS Qxy (210) peak | Qxy = 1.66 Angstrom^-1 | — | — | Text Exact Reported | 18192 · Results and Discussion · Figure 3c |
| hexagonal unit-cell lattice parameter a | a = b = 7.57 Angstrom | — | — | Text Exact Reported | 18192 · Results and Discussion · Figure 3e |
| GIWAXS FWHM for (001) peak | 0.024 Angstrom^-1 | — | — | Caption Exact Reported | SI p17 · Figure S11 caption · Figure S11b |
| GIWAXS FWHM for (100) peak | 0.020 Angstrom^-1 | — | — | Caption Exact Reported | SI p17 · Figure S11 caption · Figure S11a |
| GIWAXS FWHM for (200) peak | 0.026 Angstrom^-1 | — | — | Caption Exact Reported | SI p17 · Figure S11 caption · Figure S11c |
| GIWAXS FWHM for (210) peak | 0.025 Angstrom^-1 | — | — | Caption Exact Reported | SI p17 · Figure S11 caption · Figure S11d |