Spectroscopy — Ammonia-Assisted Chemical Vapor Deposition Growth of Two-Dimensional Conjugated Coordination Polymer Thin Films

Measurement evidence

Spectroscopy

Ammonia-Assisted Chemical Vapor Deposition Growth of Two-Dimensional Conjugated Coordination Polymer Thin Films · Liu J., Fu S., Fu Y. et al. · Journal of the American Chemical Society · 2025 · 18190-18196

4 measurement groups · 6 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

UV-Vis spectroscopy / Tauc plot

Fe-HHB-o CVD thin film without NH3 · Thin Film

Fe-HHB-o thin film directly grown on quartz substrate.

Temperature
about 298
Geometry
thin film on quartz
Context
pristine no-NH3 control film
Measurement source
SI p22 · Figure S16 · Figure S16
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
optical bandgap from Tauc plot1.11 eVCaption
Exact Reported
SI p22 · Figure S16 · Figure S16b

UV-Vis spectroscopy / Tauc plot

Fe-HHB-w NH3-assisted CVD thin film · Thin Film

Fe-HHB-w thin film directly grown on quartz substrate.

Temperature
about 298
Geometry
thin film on quartz
Context
pristine NH3-assisted target film
Measurement source
SI p22 · Figure S16 · Figure S16
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
optical bandgap from Tauc plot1.35 eVCaption
Exact Reported
SI p22 · Figure S16 · Figure S16b

XPS N 1s analysis

Fe-HHB-w-AT high-concentration NH3 treated film · Thin Film

High-concentration NH3-treated Fe-HHB-w-AT sample analysed by XPS N 1s.

Temperature
about 298
Atmosphere
ultrahigh vacuum
Geometry
treated thin film
Context
NH3-treated mechanistic sample
Measurement source
SI p28 · Figure S22 · Figure S22
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
N 1s Fe-NH3 coordination peak~399.7 eVText
Approximate
SI p28 · Figure S22 discussion · Figure S22a
N 1s NH4+ peak~401.8 eVText
Approximate
SI p28 · Figure S22 discussion · Figure S22a

XPS C 1s component analysis

Fe-HHB-w NH3-assisted CVD thin film · Thin Film

C 1s XPS comparison of Fe-HHB-w and Fe-HHB-o; reported ratios included as separate results.

Temperature
about 298
Atmosphere
ultrahigh vacuum
Geometry
thin films transferred to ESCALAB 250Xi chamber
Context
Fe-HHB-w target compared against Fe-HHB-o control
Measurement source
SI p23 · Figure S17 · Figure S17
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
C=O:C-O XPS ratio for Fe-HHB-o~1.56:1Caption
Approximate
SI p23 · Figure S17 caption · Figure S17b
C=O:C-O XPS ratio for Fe-HHB-w~1.28:1Caption
Approximate
SI p23 · Figure S17 caption · Figure S17a