Microscopy Morphology — Ammonia-Assisted Chemical Vapor Deposition Growth of Two-Dimensional Conjugated Coordination Polymer Thin Films

Measurement evidence

Microscopy Morphology

Ammonia-Assisted Chemical Vapor Deposition Growth of Two-Dimensional Conjugated Coordination Polymer Thin Films · Liu J., Fu S., Fu Y. et al. · Journal of the American Chemical Society · 2025 · 18190-18196

2 measurement groups · 8 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

AFM topography

Fe-HHB-w NH3-assisted CVD thin film · Thin Film

AFM thickness and roughness measurements for Fe-HHB-w thin films grown for 10 min to 6 h.

Temperature
about 298
Atmosphere
room temperature
Geometry
thin film on substrate
Context
pristine NH3-assisted target film
Measurement source
SI p11-12 · Figures S5-S6 · Figures 2f, S5, S6
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
surface roughness Rq for 633 nm film~8 nmText
Approximate
SI p12 · Figure S6 discussion · Figure S6
film thickness after 0.5 h growth~72.2 nmCaption
Approximate
SI p11 · Figure S5 caption · Figure S5d
film thickness after 10 min growth~11.5 nmCaption
Approximate
18191 · Results and Discussion · Figure 2f
film thickness after 1 h growth~150.8 nmCaption
Approximate
SI p11 · Figure S5 caption · Figure S5e
film thickness after 6 h growth~633.2 nmCaption
Approximate
SI p11 · Figure S5 caption · Figure S5f

HR-TEM with FFT / SAED

Fe-HHB-w NH3-assisted CVD thin film · Thin Film

Scraped Fe-HHB-w fragments transferred to copper grids and imaged by TEM.

Temperature
about 298
Atmosphere
TEM vacuum
Context
pristine NH3-assisted target film
Measurement source
18192 · Results and Discussion · Figure 3a; Figure S8
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
(100) plane distance~6.6 AngstromCaption
Approximate
18192 · Results and Discussion · Figure 3a
single-crystal region area~11750 nm2Caption
Approximate
SI p14 · Figure S8 caption · Figure S8
crystal grain/domain area~10^4 nm2Text
Approximate
18191-18192 · Results and Discussion · Figure 3a; Figure S8