Diffraction Structure — Synthesis of a highly conductive coordination polymer film via a vapor-solid phase chemical conversion process

4 measurement groups · 11 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Ag5BHT thin films · Thin Film

TEM/HR-TEM/SAED at 120 kV per SI characterisation conditions.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
HR-TEM lattice fringe d-spacing 2	d = 4.6 A	—	—	Text Rounded Reported	8722 · Results · Fig. 2d
HR-TEM lattice fringe d-spacing 1	d = 7.7 A	—	—	Text Rounded Reported	8722 · Results · Fig. 2d
SAED pattern assignment	regularly spaced diffraction spots assignable to crystal indices	—	—	Text Qualitative	8722 · Results · Fig. 2e

Ag2O film without H6BHT · Thin Film

PXRD after exposing Ag2O film without evaporated H6BHT to isopropanol post-reaction conditions.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Ag2O-only film reduction control	Ag2O films without H6BHT were reduced to Ag by isopropanol	—	—	Text Qualitative	8721-8722 · Results · Fig. S6

Scraped Ag5BHT thin-film powder · Powder

PXRD on Ag5BHT obtained by repeatedly scraping off the thin film; 2-60 deg scan range at 0.026 deg s^-1 per SI.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Absence of Ag2O and H6BHT PXRD peaks	no peaks corresponding to Ag2O and H6BHT	—	—	Text Qualitative	8721 · Results · Fig. 2b
Ag5BHT PXRD peak assigned to (020)	19.5 deg 2theta	—	—	Text Rounded Reported	8721 · Results · Fig. 2b
Ag5BHT PXRD peak assigned to (110)	11.5 deg 2theta	—	—	Text Rounded Reported	8721 · Results · Fig. 2b
Ag5BHT PXRD peak assigned to (220)	23.2 deg 2theta	—	—	Text Rounded Reported	8721 · Results · Fig. 2b
Ag5BHT PXRD peak assigned to (330)	35.2 deg 2theta	—	—	Text Rounded Reported	8721 · Results · Fig. 2b
Ag5BHT PXRD peak assigned to (50-1)	31.6 deg 2theta	—	—	Text Rounded Reported	8721 · Results · Fig. 2b

Crystalline Ag5BHT powder from vapour-solid conversion · Powder

PXRD comparison of solvent-phase Ag5BHT powder, vapour-solid Ag5BHT powder, H6BHT ligand, and Ag2O.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Vapour-solid powder phase assignment	crystalline Ag5BHT powder prepared by vapour-solid phase chemical conversion	—	—	Caption Qualitative	SI p003 · Results and Discussion · Fig. S3