Microscopy Morphology — Synthesis of a highly conductive coordination polymer film via a vapor-solid phase chemical conversion process

4 measurement groups · 11 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Ag5BHT thin films · Thin Film

SEM/EDS mapping of Ag5BHT thin films; Table S1 reports S/Ag atom ratios.

Context: pristine Ag5BHT thin film
Measurement source: SI p007-SI p008 · Results and Discussion · Fig. S9, Table S1

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
S/Ag atom ratio replicate 1	1.41:1	—	—	SI Table Exact Reported	SI p007-SI p008 · Results and Discussion · Table S1
S/Ag atom ratio replicate 2	1.58:1	—	—	SI Table Exact Reported	SI p007-SI p008 · Results and Discussion · Table S1
S/Ag atom ratio replicate 3	1.66:1	—	—	SI Table Exact Reported	SI p007-SI p008 · Results and Discussion · Table S1
Average S/Ag atom ratio	1.55:1	—	—	SI Table Exact Reported	SI p007-SI p008 · Results and Discussion · Table S1

Ag5BHT thin films · Thin Film

Physically scratched regions measured with Standard Scan, 6 s scan duration, 300 um scan length, 0.166482 um scan resolution.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Ag5BHT film thickness after conversion	292.18 nm	—	—	Text Exact Reported	8721 · Results · Fig. S5
Controllable Ag5BHT thin-film thickness range	100-300 nm	—	—	Text Range	8720 · Abstract
Ag2O/H6BHT precursor stack thickness before reaction	223.74 nm	—	—	Text Exact Reported	8721 · Results · Fig. S5
Ag5BHT thickness versus initial Ag2O thickness	linear relationship	—	—	Text Qualitative	8721 · Results · Fig. 2a

Ag5BHT thin films · Thin Film

SEM of Ag2O/H6BHT precursor interfaces, converted Ag5BHT thin films, and film folds.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Ag5BHT thin-film edge folds	some folds at the edges	—	—	Text Qualitative	8722 · Results · Fig. S8
Ag5BHT thin-film SEM morphology	homogeneous thin films composed of crystalline nanoparticles	—	—	Text Qualitative	8722 · Results · Fig. 2c

Crystalline Ag5BHT powder from vapour-solid conversion · Powder

SEM at 10 kV per SI characterisation conditions.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Vapour-solid Ag5BHT powder SEM morphology	crystalline powder particles/rods visible by SEM	—	—	Visual Estimate Qualitative	SI p004 · Results and Discussion · Fig. S4